A process for preparing relief images, comprising the steps of:
- imagewise irradiating a light-sensitive material comprised of a support and a light-sensitive layer which consists essentially of
- (a) a compound which has at least one C--O--C bond which is cleavable by acid;
- (b) a compound which forms a strong acid on irradiation, and
- (c) a binder which is insoluble in water and soluble in aqueous-alkaline solutions to produce imaged and non-imaged areas;
- warming the irradiated material in heated air to an elevated temperature sufficient to render the imaged areas resistant to developing;
- bringing the material to a lower temperature;
- uniformly irradiating the entire area of the layer;
- and
- selectively developing the non-imaged areas from the imagewise irradiating step.