Multisample dynamic headspace sampler
AssigneeSeagate Technology LLC
InventorsKarl H. Scheppers, Gregory I. Rudd
Life of this patent
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AssigneeSeagate Technology LLC
InventorsKarl H. Scheppers, Gregory I. Rudd
Estimating the term…
Method and apparatus for collecting a large number of outgas samples at the same time. Specimens to be tested for outgassing are placed in throw-away widemouth bottles, and the bottles are placed in cups provide in a heating block. A custom made cap is fastened to each bottle using an O-ring. Each cap is provided with an outgassing sample collecting tube. A source of pure gas such as nitrogen or helium is connected by way of a pressure regulator and a hydrocarbon filter to a manifold. Each of the caps on each bottle is coupled to the manifold by way of a metering valve. An adsorbent is placed in each collecting tube. The gas pressure is set to between 10 and 15 psi. The flow through each collecting tube is set to a predetermined level by adjusting its metering valve and measuring the flow at the exit of the collecting tube using a flowmeter. The healing block is heated by means of a thermal tape used in conjunction with a power supply and a thermocouple inserted into a hole in the heating block. The samples are heated and held at an elevated temperature for a predetermined length of time. After the outgassing test is completed, the collecting tubes are desorbed and analyzed with the appropriate instrumentation.
A manifold for a multichamber dynamic headspace sampler comprising:
A manifold for an outgas test fixture for simultaneously sampling off-gassed organic compounds from a plurality of specimens in a plurality of sample chambers disposed in a heater block, said manifold comprising:
A manifold for an outgas test fixture for simultaneously sampling off-gassed organic compounds from a plurality of specimens in a plurality of sample chambers disposed in a heater block, said manifold comprising:
Dependencies are inferred from the claim text.