A process for removing iodide compounds from a liquid composition comprising a carboxylic acid having 2 to 6 carbon atoms or an anhydride thereof, and metal ion contaminants, which process comprises contacting said liquid composition with a metal-exchanged ion exchange resin having strong acid cation exchange sites at least 1% of which are occupied by at least one metal selected from the group consisting of silver, mercury, palladium and rhodium wherein prior to contacting with said metal-exchanged resin, said liquid composition is contacted with a cation exchanger in the acid form to remove at least a portion of said metal ion contaminants.