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US 4,395,530 AGranted
Catalyst initiated prepolymer systems
AssigneeColamco, Inc.
InventorJames A. Hammond
Life of this patent
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Abstract
A process for the manufacture of a polyurethane prepolymer adhesive by a catalyst initiated reaction of polyol and isocyanate copolymers is performed under room temperature conditions, and in convenient quantities for application, storage, and transportation purposes. Compounding includes alternatives of catalyst and co-catalyst combinations, and additives, including a reaction inhibitor, plasticizer, delayed reaction catalyst and surfactant.
Claims30
A process for manufacturing a polyurethane prepolymer adhesive under room temperature conditions comprising the steps of:
- (a) introducing a predetermined amount of at least one polyol reactant into a reaction vessel;
- (b) mixing a predetermined amount of least one isocyanate reactant into the reaction vessel to give a uniform resin mixture sufficient to give an excess active isocyanate content in the polyurethane prepolymer adhesive of approximately 5% to 20% by weight;
- (c) adding a predetermined amount of catalyst to initiate reaction of the reactants in the reaction vessel, with vigorous stirring to give a uniform mixture, said predetermined amount of catalyst being sufficient to allow the reaction to substantially reach completion within 2 to 8 hours;
- (d) isolating the mixed contents in the reaction vessel from ambient conditions to prevent contamination of the contents by ambient moisture;
- and
- (e) mixing the reactants during the reaction in the reaction vessel until the reaction substantially subsides, whereby the polyurethane prepolymer adhesive is formed.
3 more elements
Dependencies are inferred from the claim text.