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US 4,028,485 AGranted
Non-aqueous removal of soluble hydrogenation catalyst
AssigneeMobil Oil Corporation
InventorsAnthony Poloso, James Gordon Murray
Life of this patent
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Abstract
A process for readily removing hydrogenation catalyst residue from solutions of hydrogenated olefins or olefinic polymers containing same comprising treating such solutions with non-aqueous acid followed by neutralization with anhydrous base and filtration.
Claims10
A process for the removal of hydrogenation catalyst residue, wherein said hydrogenation catalyst was formed by mixing (a) a C.sub.1 -C.sub.8 alkylaluminum or a C.sub.1 -C.sub.8 alkyllithium compound and (b) an organonickel compound of the following formula:
- ##STR2## where R is hydrogen or C.sub.1 -C.sub.12 alkyl or cycloalkyl, from a solution containing said hydrogenation catalyst and from about 1 to 50 wt. % of a hydrogenated olefinic polymer in a hydrocarbon solvent, said process comprising contacting said solution with a non-aqueous organic acid followed by neutralization with anhydrous base and filtration of said solution, thereby removing said hydrogenation catalyst residue.
Dependencies are inferred from the claim text.