Process for stable phase III potassium nitrate and articles prepared therefrom
AssigneeTechnovation, Inc.
InventorGeorge A. Rohrer
Life of this patent
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Abstract
A ferroelectric Phase III potassium nitrate (KNO.sub.3) which is stable at ambient temperatures is produced in accordance herewith by crystallizing reagent grade KNO.sub.3 under vacuum and heat and, then, equilibrating the resultant to ambient conditions. This stable Phase III KNO.sub.3 which is of crystalline structure exhibits visual and optical effects when subjected to mechanical and electrical alteration of the polarization vector of the crystalline structure, thus, rendering it useful in the manufacture of transparent electrodes by interposing this crystalline material between the electrodes, and the like. Furthermore, ferroelectric thin film memory arrays can be produced herefrom.
Claims6
A process for the preparation of a Phase III potassium nitrate which is stable at ambient conditions, comprising:
- a. melting reagent grade potassium nitrate in the presence of a vacuum having a maximum pressure of about 1 .times. 10.sup.-.sup.5 torr,
- b. evaporating the melted potassium nitrate at a temperature of from about 390.degree. C to 440.degree. C while maintaining the vacuum,
- c. collecting the vapors in the form of a thin film of Phase III potassium nitrate, and
- d. relieving the vacuum to atmospheric pressure and allowing the temperature to reach room temperature while maintaining a moisture-free atmosphere.
A process of manufacturing a ferroelectric device comprising the steps of:
- forming a first electrical contact;
- forming, by vapor deposition performed in a vacuum at a pressure no greater than 1 .times. 10.sup.-.sup.5 torr and at a temperature of from about 390.degree. C to 440.degree. C, a stable thin film of potassium nitrate over at least a portion of said first electrical contact;
- relieving said vacuum to a pressure of approximately one atmosphere with a dry predetermined gas for a predetermined period of time;
- reapplying said vacuum;
- and
- forming a second electrical contact over at least a portion of said stable thin film of potassium nitrate.
Dependencies are inferred from the claim text.