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US 2024/0384030 A1Published application
Method for preparation of polytrimethylene ether glycol and polytrimethylene ether glycol using the same
AssigneeSK Chemicals Co., Ltd.
InventorsHan-Gyeol CHO, Jae-Il CHUNG, Hyun Jun CHO
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Abstract
This invention relates to a method for preparing polytrimethylene ether glycol having excellent properties, by improving purification efficiency using an organic solvent in the hydrolysis step, and polytrimethylene ether glycol prepared thereby.
Claims17
A method for preparing polytrimethylene ether glycol comprising steps of:
- conducting condensation polymerization of diol monomers in the presence of an acid catalyst to prepare a polymerization product (step 1);
- hydrolyzing the polymerization product using an organic solvent and water to prepare a hydrolyzed mixture (step 2);
- neutralizing the hydrolyzed mixture using basic salt (step 3);
- separating an aqueous phase and an organic phase after neutralization (step 4);
- and
- filtering salts existing in the organic phase (step 5).
3 more elements
Polytrimethylene ether glycol wherein the number average molecular weight is 1000 to 5000 g/mol, and
- miliequivalent of base per 30 kg of polytrimethylene ether glycol is 3 or less.
Dependencies are inferred from the claim text.