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US 2024/0368835 A1Published application
Grinding method and grinding medium
OwnerLewis TAYLOR, Chris BONDS +3inventors
InventorsLewis TAYLOR, Chris BONDS, Paymaan TAHAMTAN, Ben BULSON, David Robert SKUSE
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Abstract
An improved grinding method for manufacturing microfibrillated cellulose.
Claims34
A method for preparing microfibrillated cellulose having at least one of increased tensile properties and reduced media wear, the method comprising:
- providing a suspension comprising pulp fibres in a liquid medium, wherein the fibre solids content of the suspension is about 0.3 wt % to about 4 wt %;
- microfibrillating the pulp fibres by grinding the suspension in the presence of a grinding medium in one or more wet stirred media mills, wherein:
- the grinding medium comprises about 0.5 mm to about 12 mm particles,
- the grinding medium has an arithmetic surface roughness from about 0.02 μm to about 2 μm,
- the media volume concentration of the grinding medium is about 30% to about 65% of the total volume of the charge of the one or more wet stirred media mills,
- the grinding is performed with an energy input of less than about 6,000 kWh/t, and
- grinding the suspension results in a worn media content of less than about 20% by dry mass;
- and
- recovering the microfibrillated cellulose from the one or more wet stirred media mills.
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Dependencies are inferred from the claim text.