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US 2024/0367230 A1Published application
Method of making max phase structures
AssigneeUchicago Argonne, LLC
InventorsDileep Singh, Beihai Ma
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Abstract
A method of forming MAX phase structures having one or more apertures includes filing a green body having one or more apertures with an insert powder and sintering while applying a load to the insert filled green body to from the MAX phase structure.
Claims26
A method of making a MAX phase structure comprising one or more apertures:
- forming precursor powder into a green body structure having one or more apertures;
- filling the one or more apertures with an insert powder such that the insert powder completely fills the one or more apertures;
- sintering the insert powder filled green body while applying a pressure load from a pressure applying insert applied to the insert powder filled green body thereby form the MAX phase structure;
- wherein:
- the MAX phase structure comprises a MAX phase compound of formula Mn+1AXn, wherein n is 1-4, wherein M is an early transition metal element, A is an A-group metal, and X is carbon or nitrogen,
- the precursor powder comprises a powder of M, a powder of A, and one or both of a powder of a carbide of M and a powder of a nitride of M, and
- the insert powder comprises a material that does not sinter at a temperature at which the green body is sintered.
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Dependencies are inferred from the claim text.