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US 2024/0351889 A1Published application
Method for producing silica particles, silica particles produced by such method, compositions and uses of such silica particles
AssigneeMerck Patent GmbH
InventorsEric JACQUINOT, Leo HANUS, Geary GRAHAM
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Abstract
The present application relates to a method for producing silica particles, and to the silica particles produced by such method. The present application further relates to compositions comprising the silica particles produced by such method as well as to uses of such silica particles and compositions comprising such silica particles.
Claims17
Method for the production of silica particles, said method comprising the steps of
- (a) hydrolyzing a silicon chloride in aqueous solution, thereby producing a gel comprising silicic acid and hydrogen chloride, wherein the silicon chloride is of the following formula (1′)
- RcSi(OH)dCl4-c-d (1′)
- with R being at each occurrence independently selected from the group consisting of alkyl groups having 1, 2, or 3 carbon atoms;
- and c being at each occurrence independently selected from the group consisting of 0, 1, 2, and 3;
- and d being at each occurrence independently selected from the group consisting of 0, 1, 2, and 3;
- provided that c+d≤3;
- (b) removing at least part of the hydrogen chloride from the gel to obtain a purified gel;
- (c) adjusting the pH of the purified gel to at least 9;
- and
- (d) then polycondensating silicic acid to form the silica particles.
7 more elements
Dependencies are inferred from the claim text.