Process for the synthesis, with multiple seeding, of zeolite crystals having a controlled particle size
AssigneeArkema France
InventorsSerge Nicolas, Cécile Lutz
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Abstract
The present invention relates to a process for preparing zeolite crystals having a multimodal particle size distribution, and the sizes of which are between 0.02 μm and 20 μm, said process comprising a first introduction of one or more seeding agents into the tubular reactor or upstream of the tubular reactor, and at least one second introduction of one or more, identical or different, seeding agents into the tubular reactor.
Claims10
Process for preparing zeolite crystals having a multimodal particle size distribution, and the sizes of which are between 0.02 μm and 20 μm, said process comprising at least the following steps:
- a) preparing a synthesis gel by mixing at least one source of silica, at least one source of alumina and optionally, at least one aqueous alkali or alkaline-earth metal hydroxide solution,
- b) feeding a tubular reactor with said synthesis gel,
- c) first introduction of one or more seeding agents into the tubular reactor or upstream of the tubular reactor,
- d) second introduction of one or more, identical or different, seeding agents into the tubular reactor,
- e) carrying out the crystallization reaction, in the tubular reactor, of the synthesis gel in the presence of the seeding agent(s), forming the reaction medium,
- f) filtering the reaction medium in order to recover crystals produced.
Dependencies are inferred from the claim text.