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US 2021/0002177 A1Published application
Ceramic material and method of preparing the same
AssigneeUniversity of Electronic Science and Technology of China
InventorsEnzhu LI, Hongcheng YANG, Chengli SUN, Chaowei ZHONG, Shuren ZHANG
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Abstract
A ceramic material, including: BaWO4-xM2CO3-yBaO-zB2O3-wSiO2, where x=0-0.2 mole, y=0-0.05 mole, z=0-0.2 mole, w=0-0.1 mole, M represents an alkali metal ion selected from Li+, K+, Na+, and x, y, z, and w are not zero at the same time.
Claims3
A ceramic material, comprising:
- BaWO4-xM2CO3-yBaO-zB2O3-wSiO2, wherein x=0-0.2 mole, y=0-0.05 mole, z=0-0.2 mole, w=0-0.1 mole, M represents an alkali metal ion selected from Li+, K+, Na+, and x, y, z, and w are not zero at the same time.
A method, comprising:
- 1) weighing and mixing BaCO3, WO3, M2CO3, B2O3 and SiO2 based on a chemical formula BaWO4-xM2CO3-yBaO-zB2O3-wSiO2, wherein x=0-0.2 mole, y=0-0.05 mole, z=0-0.2 mole, w=0-0.1 mole, M represents an alkali metal ion selected from Li+, K+, Na+, and x, y, z, and w are not zero at the same time, to yield a first powder;
- 2) mixing the first powder obtained in 1), zirconia balls, and deionized water according to a mass ratio of 1:5:1-2, ball-milling for 4-7 h, drying at 80-120° C., sieving with a 40-60 mesh sieve, calcining in air atmosphere at 700-900° C. for 2-4 h, to yield a second powder;
- 3) mixing the second powder obtained in 2), zirconia balls, and deionized water according to a mass ratio of 1:5:1-2, ball-milling for 3-6 h, drying, to yield a third powder, and adding a binder to the third powder;
- and
- 4) compression molding a resulting product obtained in 3) under a pressure of 20 megapascal, drying at 400-500° C. and sintering at 850° C.-900° C. for 0.5-2 h.
2 more elements
Dependencies are inferred from the claim text.