Method for Preparing Lithium Bis(Fluorosulfonyl)imide Salt
AssigneeLG Chem, Ltd.
InventorsByung Soo Kang, Hyun Jik Lee, Won Jae Lee, Chul Haeng Lee, Young Min Lim
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AssigneeLG Chem, Ltd.
InventorsByung Soo Kang, Hyun Jik Lee, Won Jae Lee, Chul Haeng Lee, Young Min Lim
Estimating the term…
The present invention relates to a method for preparing a lithium bis(fluorosulfonyl)imide salt, including a step of dissolving bis(chlorosulfonyl)imide in an organic solvent in a non-glass vessel to prepare a first reaction solution; a step of injecting lithium fluoride (LiF) to the first reaction solution in the non-glass vessel and refluxing while heating to prepare a second reaction solution; a step of separating a product including a lithium bis(fluorosulfonyl)imide salt and the organic solvent from the second reaction solution; and a step of obtaining the lithium bis(fluorosulfonyl)imide salt in a solid phase from the product, wherein the organic solvent is at least one or more selected from the group consisting of ethyl acetate, butyl acetate, chloroform, dichloromethane, dichloroethane, benzene, xylene and acetonitrile.
A method for preparing a lithium bis(fluorosulfonyl)imide salt, the method comprising:
Dependencies are inferred from the claim text.