A coal and oil co-hydrotreating processing technology and equipment
AssigneeCatech Technology Co., Ltd.
InventorSuan LI
Life of this patent
Estimating the term…
Abstract
An oil-coal co-hydrotreating processing includes the following steps: pulverized coal, vacuum residue and recycle oil are mixed to prepare coal slurry. After mixed with hydrogen, catalyst and additive, oil-coal slurry is preheated into a slurry bed reactor with high reacting pressure for thermal cracking and hydrogenation reaction. After reaction, all the products go into the hot high pressure separator for separation of solid from the bottom and gas from the top. The gas obtained goes into the fixed bed reactor for further hydrocracking or refining, and the distillate obtained enter the fractionating tower. The vacuum gas oil from the bottom of fractionating tower is taken as recycle oil piped to the oil-coal slurry mixing device as solvent.
Claims10
A oil-coal co-hydrotreating processing technology, characterized as the following steps:
- first of all, pulverizing the coal and drying, wherein the pulverized coal is mixed with one or several of crude oil, atmospheric residue, vacuum residue, FCC slurry oil, deasphalted oil, vacuum gas oil, coal tar in the coal and oil mixing and pulping device to prepare oil-coal slurry;
- after mixed with hydrogen, catalyst and additive, the oil-coal slurry is preheated into a slurry bed reactor with reacting pressure for thermal cracking and hydrogenation reaction;
- the coke, asphaltene and heavy metals are adsorbed on the catalyst, additives and unreacted coal in the reaction process;
- after reaction, all the products go into the hot high pressure separator for separation of solid from the bottom and gas from the top, and the gas goes into the fixed bed reactor for further hydrocracking or refining;
- distillate obtained enters the fractionating tower, and bottom vacuum gas oil is recycled to the coal and oil mixing and pulping device;
- wherein the catalyst is a mixture of molybdate and iron, the additive is a sulfurizing reagent, and the reaction pressure in the slurry bed reactor is in the range of 17-20 MPa.
A coal and oil co-hydrotreating equipment, characterized as the oil-coal slurry conveying pipe of the coal and oil mixing and pulping device is first connected with the adding device of catalyst and additive, and then combined with hydrogen pipeline and connected with the furnace then the pipeline for transportation of oil-coal slurry/catalyst/additive/hydrogen mixture from the furnace is connected with the slurry bed reactor and the slurry bed reactor is connected with the hot high pressure separator and wherein the upper part of the hot high pressure separator is connected with a fixed bed reactor and the bottom is connected with the vacuum flash tower;
- the fixed bed is further connected to the cold high pressure separator whose top is connected with a gas purification device, and bottom is connected with a fractionating tower;
- there are only medium distributors arranged in the internal of the slurry bed reactor but no support plate of bed, and the inner wall is ceramic;
- the vacuum gas oil from the fractionation tower is connected with the coal and oil mixing and pulping device.
Dependencies are inferred from the claim text.