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US 2018/0023005 A1Published application
Device and process for the recovery of increased volumes of pure terpenes and terpenoids from scrap polymers and elastomers
OwnerEarl R. Beaver, Jonathan L. Wistrominventors
Life of this patent
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Abstract
A device and process for the vacuum pyrolization of scrap tires to produce a pyrolytic oil from which valuable terpenes such as limonene and pulegone may be extracted and purified.
Claims18
A device for the pyrolysis of tires to form pyrolytic oils containing limonene and pulegone comprising;
- a nitrogen blanket bin for accepting shredded, washed, and dried automobile tires;
- at least one vacuum-lock valve;
- a helical screw which slowly turns to generate a mixture of shredded automobile tires and an additive/catalyst that can flow from the nitrogen blanket bin;
- at least one heater for heating the mixture from ambient temperature to about 450 degrees Celsius;
- a release valve for controlling the release of at least one of either a material and a vapor from the nitrogen blanket vacuum sealed furnace through a thin film evaporator and into a contactor/separator for recovery of at least one of either a type of terpene or a type of terpenoid from a mixture that has at least one of either the material or the vapor, wherein the contactor/separator can generate a pyrolytic vapor from the at least one of either the material or the vapor after a set of solids is removed from the mixture, and wherein the contactor/separator includes a chiller assembly for reducing the temperature of the pyrolytic vapor, a first heatable distillation column for reheating and cooling the mixture, a second heatable distillation column containing internal components that are at least one of either sieve trays or structured packing, wherein the second distillation column separates types of terpenes and the types of terpenoids that have been extracted from the mixture, wherein the mixture is passed through a small orifice disposed between the first distillation column and the second distillation column to thereby reduce the temperature of the mixture as it enters the second distillation column, wherein the terpenes and terpenoids are removed from the second distillation column through at least one tap mounted on an outside surface of the second distillation column, and
- a piping system for transporting the liquid and vapor products that are one of either produced, transferred, recovered, or purified by the device for the pyrolysis of tires to form pyrolytic oils containing limonene and pulegone.
3 more elements
A device for the pyrolysis of tires to form pyrolytic oils containing limonene and pulegone comprising;
- a nitrogen blanket vacuum sealed furnace for accepting automobile tires;
- a heater for heating the nitrogen blanket vacuum sealed furnace to at least about 200 degrees Centigrade;
- a vacuum pump for generating a vacuum in the nitrogen blanket vacuum sealed furnace;
- an additive/catalyst placed within the nitrogen blanket vacuum sealed furnace for dispersion over the automobile tires;
- a release valve for controlling the release of at least one of either a material and a vapor from the nitrogen blanket vacuum sealed furnace a thin film evaporator and into a contactor/separator for recovery of at least one of either a type of terpene or a type of terpenoid from a mixture that has at least one of either the material or the vapor, wherein the contactor/separator can generate a pyrolytic vapor from the at least one of either the material or the vapor after a set of solids is removed from the mixture, and wherein the contactor/separator includes a chiller assembly for reducing the temperature of the pyrolytic vapor, a first distillation column for reheating and cooling the mixture, a second distillation column containing internal components that are at least one of either sieve trays or structured packing, wherein the second distillation column separates types of terpenes and the types of terpenoids that have been extracted from the mixture, wherein the mixture is passed through a small orifice disposed between the first distillation column and the second distillation column to thereby reduce the temperature of the mixture as it enters the second distillation column, wherein the terpenes and terpenoids are removed from the second distillation column through at least one tap mounted on an outside surface of the second distillation column, and
- a piping system for transporting the liquid and vapor products that are one of either produced, transferred, recovered, or purified by the device for the pyrolysis of tires to form pyrolytic oils containing limonene and pulegone.
3 more elements
Dependencies are inferred from the claim text.