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US 2018/0022681 A1Published application
A novel process for the preparation of hydroxyl functional esters and polyesters therefrom
AssigneeCouncil of Scientific and Industrial Research
InventorsYogesh Ramesh Nevare, Susheela Bhaskar Idage, Bhaskar Bhairavnath Idage, Swaminathan Sivaram
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Abstract
The present invention relates to a novel process for the preparation of a linear monomer alkyl lactyl lactate by a simple esterification reaction of acid with ester in presence of suitable catalysts or reagents. The present invention further relates to a process for the preparation of poly acid from alkyl lactyl lactate by using suitable catalyst.
Claims9
A novel process for the preparation of a alkyl lactyl lactate comprising the following steps:
- a) stirring the reaction mixture of alkyl lactate, condensing reagents in anhydrous solvent at 0° C.;
- b) adding a solution of acid in solvent to a reaction mixture of step (a) slowly over a period of 1 to 3 hours;
- c) stirring the reaction mixture at temperature 27° C. for 10 to 12 hours to afford the product of monomer of alkyl lactyl lactate.
Dependencies are inferred from the claim text.