PROCESS FOR IN SITU SYNTHESIS OF DISPERSION ZnO NANOPARTICLES IN OIL
AssigneeIndian Oil Corporation Limited
InventorsMunusamy VIJAYARAJ, Samik Kumar HAIT, Madhira Indu Sekhara SASTRY, Sankara Sri Venkata RAMAKUMAR
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Abstract
The present invention relates to a process for synthesizing dispersion of ZnO nanoparticles in an oil medium. Particularly, the invention relates to a process for in-situsynthesis of dispersion of ZnO nanoparticles in oil medium. Additionally, the present invention relates to a lubricant oil composition, wherein the composition comprises a base oil, a dispersant and the dispersion of ZnO as obtained by the process of the present invention.
Claims18
A process for in situ synthesis of dispersion of Zno nanoparticles in an oil additive composition, wherein the process comprises the steps of dissolving a zinc salt in an alcoholic solvent and heating to 60-120° C. for 6-48 h hours to obtain a suspension;
- a) centrifuging the suspension as obtained in step (a) and washing with deionized water to obtain a precipitate of layered base zinc (LBZ);
- b) dispersing the layered base zinc precipitate as obtained step (b) in an alcohol and adding to base oil containing a dispersant;
- c) refluxing the mixture to obtain a colloidal suspension;
- evacuating the colloidal suspension at room temperature and heating at 60-90° C., followed by heating to 90-140° C. for 45 to 120 minutes to obtain a dispersion of ZnO in the oil medium.
Dependencies are inferred from the claim text.