Fluidized bed reactor and method for producing granular polysilicon
AssigneeWacker Chemie AG
InventorsDirk WECKESSER, Harald HERTLEIN
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AssigneeWacker Chemie AG
InventorsDirk WECKESSER, Harald HERTLEIN
Estimating the term…
Granular polysilicon is produced in a fluidized-bed reactor by fluidizing silicon particles by means of a gas flow in a fluidized bed heated to a temperature of 850-1100° C., adding a silicon-containing reaction gas by means of a nozzle and depositing of silicon on the silicon particles, wherein, in at least 56% of an axially symmetric region around a nozzle opening of the nozzle, the reaction gas concentration is greater than 75% of the maximum concentration of the reaction gas (10 to 50 mol %), the fluidized-bed temperature is greater than 95% of the fluidized-bed temperature outside the axially symmetric region (850-1100° C.) and the solids concentration is greater than 85% of the solids concentration at the edge of the fluidized bed (55 to 90% by volume).
-9. (canceled)
A method for producing granular polysilicon in a fluidized-bed reactor, comprises fluidizing silicon seed particles by a hydrogen gas flow in a fluidized bed which is heated to a temperature of 850-1100° C., adding trichlorosilane as a silicon-containing reaction gas by means of at least one nozzle, wherein a local gas velocity at an outlet of the at least one nozzle is 0.5 to 200 m/s, and depositing silicon on the silicon seed particles, wherein, relative to the reactor cross sectional area, a specific mass stream of trichlorosilane is 1600-5500 kg/(h×m2), a specific hydrogen volumetric stream is 800-4000 Nm3(STP)/h×m2), a specific bed weight of the fluidized bed is 800-2000 kg/m2, a specific seed particle metering rate is 8-25 kg/(h×m2) and a specific reactor heating power is 800-3000 kW/m2, and wherein the mass stream of trichlorosilane, the hydrogen volumetric stream and the reactor heating power are selected such that in at least 56% of an axially symmetric region around a nozzle opening of the at least one nozzle;
Dependencies are inferred from the claim text.