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US 2010/0168298 A1Published application
Method for manufacturing hydrogenated block copolymer
AssigneeTSRC Corporation
InventorsHuan-Chun Kao, Sheng-Te Yang, Hung-Chieh Hou, Chung-Ming Tsai
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Abstract
The present invention relates to a method for manufacturing a substantially hydrogenated vinyl aromatic/conjugated diene block copolymer, which has a hydrogenation level of greater than 90 percent. The resulting substantially hydrogenated vinyl aromatic/conjugated diene block copolymer has advantageous physical properties suitable for use in discs, optical films, light guide plates, etc.
Claims21
A method for manufacturing a substantially hydrogenated block copolymer, comprising:
- hydrogenating a block copolymer of a vinyl aromatic polymer block and a conjugated diene polymer block by contacting with a hydrogenating agent in the presence of a hydrogenation catalyst to obtain a polymer solution including a hydrogenated block copolymer having a hydrogenation level of greater than 90 percent and a solvent;
- removing said solvent from said polymer solution by a flash devolatilization at a temperature of 200 to 300° C. and a pressure of 1 to 10 Bar to obtain a concentrated polymer solution with a residual solvent in an amount of 1 to 50 weight percent based on the total weight of said concentrated polymer solution;
- and
- removing said residual solvent from said concentrated polymer solution by a devolatilizer at a pressure below 100 torr to isolate said hydrogenated block copolymer.
1 more element
Dependencies are inferred from the claim text.