Process for preparing microrods using liquid-liquid dispersion
AssigneeNorth Carolina State University
InventorsOrlin Dimitrov Velev, Rossitza Gueorguieva Alargova
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AssigneeNorth Carolina State University
InventorsOrlin Dimitrov Velev, Rossitza Gueorguieva Alargova
Estimating the term…
The invention provides a method for forming polymer microrods, the method including the steps of providing a polymer solution comprising a polymer dissolved in a first solvent; providing a dispersion medium comprising a second solvent, wherein the first solvent and the second solvent are miscible or partially soluble in each other, and wherein the polymer is insoluble in the second solvent; adding the polymer solution to the dispersion medium to form a dispersed phase of polymer solution droplets within the dispersion medium; and introducing a shear stress to the dispersion medium and dispersed polymer solution droplets for a time and at a shear rate sufficient to elongate the polymer solution droplets to form microrods and solidify the microrods by attrition of the polymer solvent into the dispersion medium.
A plurality of polymer microrods having an average aspect ratio of at least about 5, an average length of about 10 to about 100 μm, and an average diameter of about 0.1 to about 10 μm.
Dependencies are inferred from the claim text.