Low nitrogen concentration carbonaceous material and manufacturing method thereof
AssigneeToyo Tanso Co., Ltd.
InventorIchiro Fujita
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Abstract
The present invention relates to a low nitrogen concentration carbonaceous material with a nitrogen concentration according to glow discharge mass spectrometry of 100 ppm or less, as well as a manufacturing method thereof are provided. A carbonaceous material subjected to a high purification treatment in a halogen gas atmosphere is heat treated under a pressure of 100 Pa or less and at a temperature of 1800° C. or higher, releasing nitrogen in the carbonaceous material and then cooling the material under a pressure of 100 Pa or less or in a rare gas atmosphere.
Claims8
A low nitrogen concentration carbonaceous material in which a
A low nitrogen concentration carbonaceous material in which a nitrogen concentration according to glow discharge mass spectrometry is 100 ppm or less.
A method of manufacturing a low nitrogen concentration carbonaceous material, which comprises heat treating a carbonaceous material subjected to a high purification treatment in a halogen gas atmosphere, at a pressure of 100 Pa or less and at 1800° C. or higher, releasing nitrogen in the carbonaceous material, then cooling the material to a predetermined temperature at a pressure of 100 Pa or less and then cooling the same to a room temperature in a rare gas atmosphere.
A method of manufacturing a low nitrogen concentration carbonaceous material, which comprises heat treating a carbonaceous material subjected to a high purification treatment in a halogen gas atmosphere, at a pressure of 100 Pa or less and at 1800° C. or higher, releasing nitrogen in the carbonaceous material, then introducing a rare gas and then cooling the material to a room temperature in a rare gas atmosphere.
A low nitrogen concentration carbonaceous material obtained from a carbonaceous material by applying a high purification treatment in a halogen containing gas atmosphere at 2400° C. or higher and then further supplying a halogen containing gas under a reduced pressure at 2000° C. or higher, having a nitrogen concentration content of 1×1017 atoms/cm3 or less using SIMS analysis.
A method of manufacturing a low nitrogen concentration carbonaceous material which comprises applying a high purification treatment to a carbonaceous material in a halogen containing gas atmosphere at 2400° C. or higher and then further supplying a halogen containing gas under a reduced pressure at 2000° C. or higher.
Dependencies are inferred from the claim text.