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US 11,026,869 B2Granted
Process for producing small droplet emulsions at low pressure
AssigneeConopco, Inc.
InventorsDavid John Lang, Congling Quan
Life of this patent
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Abstract
The present invention relates to novel process for making oil-in-water nanoemulsions. The oil phase contains oil selected from the group consisting of triglyceride oil and/or petrolatum and a C8 to C16 fatty acid just be added during preparation; and the aqueous phase contains specific N-acyl derivatives of carboxylic amino acid as primary emulsifier.
Claims13
A process for making a nanoemulsion composition comprising:
- a) an internal phase comprising (i) 55 to 75% by wt. of total nanoemulsion composition of oils selected from the group consisting of triglyceride, petrolatum and mixtures thereof, wherein the melting point of the petrolatum is 30 to 60° C.;
- and (ii) 1.1 to 8% by wt. nanoemulsion of a C8 to C18 fatty acid;
- and
- b) an external aqueous phase comprising 2 to 15% by wt. of total nanoemulsion composition of a surfactant or surfactants which are N-acyl derivatives of amino acid salt;
- wherein the surfactant of (b) comprises 50% or greater of all surfactant present in said external aqueous phase;
- wherein the volume average diameter of droplets of (a) is 20 to 600 nanometers,
- wherein said process comprises:
- 1) adding the C8 to C18 fatty acid of component (a)(ii) to oil of (a)(i);
- 2) heating oil phase (a) to a sufficient temperature so that all compounds are molten;
- and
- 3) Heating the aqueous phase to a temperature range of 45 to 75° C.;
- and
- 4) Simultaneously pumping the heated aqueous and oil phases via a sonolator or a conventional homogenizer using process pressure of 500 pounds per square inch (psi) or less.
10 more elements
Dependencies are inferred from the claim text.