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US 10,865,177 B2Granted
Process for making high purity salts
AssigneeMilliken & Company
InventorsDarin L. Dotson, Xiaoying Wang, Rui Liu
Life of this patent
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Abstract
A process for making a high purity salt comprises the steps of providing an organic compound, providing a metal salt, adding the metal salt and organic compound to an aqueous medium, heating the reaction mixture to react the organic compound and the metal salt to form an organic salt, collecting the organic salt, exposing the collected organic salt to microwave radiation, and exposing the collected organic salt to infrared radiation.
Claims10
A process for making a high purity salt, the process comprising the steps of:
- (a) providing an organic compound selected from the group consisting of cis-cyclohexane-1,2-dicarboxylic acid anhydride, cis-cyclohexane-1,2-dicarboxylic acid, and mixtures thereof;
- (b) providing a metal salt selected from the group consisting of metal hydroxides and metal carbonates, the metal salt comprising a metal selected from the group consisting of alkali metals and alkaline earth metals;
- (c) adding the metal salt and the organic compound to an aqueous medium to produce a reaction mixture;
- (d) heating the reaction mixture to a temperature of about 65° C. to about 80° C. to react the organic compound and the metal salt and form an organic salt;
- (e) collecting the organic salt from the aqueous medium;
- (f) exposing the collected organic salt to microwave radiation having a frequency of about 900 MHz to about 2,500 MHz to reduce the moisture content of the organic salt to about 20% or less;
- and
- (g) exposing the organic salt from step (f) to infrared radiation having a frequency of about 9.9×104 GHz to about 3×105 GHz to reduce the moisture content of the organic salt to about 7% or less.
5 more elements
Dependencies are inferred from the claim text.