Process for producing conjugated diene polymer
AssigneeAsahi Kasei Kabushiki Kaisha
InventorTetsuji Tokiwa
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Abstract
The present invention provides a process for producing a conjugated diene polymer, the process including a production step of producing a conjugated diene polymer solution containing a conjugated diene polymer and a solvent, and a devolatilization step of heating the conjugated diene polymer solution while conveying the conjugated diene polymer solution with an apparatus having rotary twin screws, thereby devolatilizing the solvent, in which a motor current value of the screw in the devolatilization step and a motor current value of the screw under no load satisfy a predetermined relational expression.
Claims14
A process for producing a conjugated diene polymer, the process comprising:
- a production step of producing a conjugated diene polymer solution comprising a conjugated diene polymer and a solvent;
- and
- a devolatilization step of heating the conjugated diene polymer solution while conveying the conjugated diene polymer solution with an apparatus comprising rotary twin screws, thereby devolatilizing the solvent,
- wherein a motor current value of the screw in the devolatilization step and a motor current value of the screw under no load satisfy following relational expression (1):
- 1.05≤((I1)/(I0))≤2.00 (1)
- wherein I1 represents the motor current value [A] of the screw in the devolatilization step and I0 represents the motor current value [A] of the screw under no load,
- wherein:
- a ratio of a screw length to a screw diameter in the apparatus is 4.0 or more and 12 or less;
- and,
- in the devolatilization step, an inner volume of the apparatus and an amount of the solvent volatilizing per unit time satisfy following relational expression (2):
- 1.0≤((VA)/(V0))≤50 (2)
- wherein (V0) represents the inner volume [L] of the apparatus and (VA) represents the amount [L] of the solvent volatilizing per unit time [h].
Dependencies are inferred from the claim text.