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US 10,246,405 B2Granted
Porous diacetylene particles, synthesis method thereof
AssigneeKorea University Research and Business Foundation
InventorsDong June Ahn, Doo Ho Yang
Life of this patent
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Abstract
Provided are a radial porous diacetylene particle, which is synthesized by ion-bonding a diacetylene-containing dicarboxylic acid or diamine monomer represented by Formula 1 with a diamine or dicarboxylic acid monomer represented by Formula 2, and a method of manufacturing the same.
Claims8
A method of manufacturing a radial porous diacetylene particle, comprising the steps of:
- (a) respectively dissolving a diacetylene-containing dicarboxylic acid monomer represented by Formula 1 below and a diamine monomer represented by Formula 2 below in a solvent to prepare a solution including the diacetylene-containing dicarboxylic acid monomer and a solution including the diamine monomer:
- G-(A)x-C≡C—C≡C—(B)y-G [Formula 1]
- wherein A and B are each independently selected from the group consisting of a substituted or unsubstituted alkyl group of two or more carbon atoms, an ethylene oxide group, an amide group and an ester group, G is COOH, and x and y are each independently an integer of 1 to 20,
- Q-(D)m-Z-(E)n-Q [Formula 2]
- wherein Z is selected from the group consisting of a benzene group, a pyridine group, a pyrimidine group and a naphthalene group, D and E are each independently a substituted or unsubstituted alkyl group of one or more carbon atoms Q, NH2, and m and n are each independently an integer of 0 to 20;
- (b) ultrasonically treating each of the solutions;
- (c) maintaining each of the ultrasonically-treated solutions at room temperature;
- and
- (d) mixing the solution including the diacetylene-containing dicarboxylic acid monomer represented by Formula 1 above with the solution including the diamine monomer represented by Formula 2 above to form a radial porous diacetylene particle and then growing the radial porous acetylene particle.
6 more elements
Dependencies are inferred from the claim text.