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US 10,119,032 B2Granted
Process for the preparation of a mineral filler product
AssigneeOmya International AG
InventorsSamuel Rentsch, Fabio Ippolito, Matthias Buri, Patrick A. C. Gane
Life of this patent
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Abstract
A process for the preparation of a mineral filler product is disclosed, the process comprising a step of wet grinding a calcium carbonate-containing material in a mixture obtained by contacting the calcium carbonate-containing material with at least one grinding agent selected from specific styrene-maleic anhydride co-polymers and/or specific derivatives of styrene-maleic anhydride co-polymers.
Claims22
A process for the preparation of a mineral filler product, the process comprising the steps of:
- a) providing a calcium carbonate-containing material;
- b) providing water;
- c) providing at least one grinding agent;
- d) wet grinding the calcium carbonate-containing material in a mixture obtained by contacting:
- i) the calcium carbonate-containing material provided in step a), with
- ii) the water provided in step b), and with
- iii) the at least one grinding agent provided in step c) in any order in at least one grinding unit to obtain a wet ground mineral filler;
- e) optionally classifying the wet ground mineral filler of step d) to obtain a coarse fraction and a fine fraction, wherein the coarse fraction is removed or subjected to wet grinding step d) and the fine fraction represents a fine mineral filler;
- f) drying the wet ground mineral filler of step d) and/or the fine mineral filler of step e) to obtain a dried mineral filler having a total moisture content of less than or equal to 1.0 wt.-%, based on the total weight of said dried mineral filler;
- and
- g) treating the dried mineral filler of step f) with a hydrophobizing agent to obtain a surface-treated product having a treatment layer on at least part of the surface of said product;
- wherein the total moisture content in the mixture of step d) ranges from 15.0 to 50.0 wt.-%, based on the total weight of said mixture;
- the amount of the at least one grinding agent provided in step c) ranges from 0.01 to 10.0 wt.-%, based on the total dry weight of the calcium carbonate-containing material;
- the temperature in step d) ranges from 60° C. to 150° C.;
- and
- the at least one grinding agent is selected from the group consisting of styrene-maleic anhydride co-polymers and derivatives of styrene-maleic anhydride co-polymers, said derivatives being selected from styrene-maleic anhydride co-polymers having partially or fully hydrolyzed maleic anhydride units, wherein said grinding agent has a monomer unit ratio (styrene units:maleic anhydride units, S:MA) of from 1:2 to 5:1 and a molecular weight MW of from 500 to 40,000 g/mol.
13 more elements
Dependencies are inferred from the claim text.