Process for producing a high tensile strength, high Young's modulus carbon fiber having excellent internal structure homogeneity
AssigneeToray Industries, Inc.
InventorYoshiro Kinoshita
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AssigneeToray Industries, Inc.
InventorYoshiro Kinoshita
Estimating the term…
High tensile strength, high Young's modulus carbon fiber, free from holes and voids having a statistical probability of holes detected by a standard plasma etching test of less than about 2%, a tensile strength of at least about 150 kg/mm.sup.2 and a Young's modulus of at least about 15.times.10.sup.3 kg/mm.sup.2. The carbon fiber has excellent homogeneity of internal structure and excellent reliability as a composite material. A process is provided for producing a high performance, high quality carbon fiber having excellent productivity and operability and requiring only a short time for oxidation. The process comprises converting an organic polymeric fiber (preferably an acrylic fiber) to an oxidized fiber, comprising repeatedly bringing said fiber into contact with the surface of a heated body such as a heated roll or heated plate at about 200.degree.-400.degree. C. in the presence of an oxidizing gas for a contact time per single contact of said fiber with the surface of the heated body of less than about 1 second, and heating the resulting oxidized fiber in an atmosphere of an inert gas at a temperature of at least about 800.degree. C. to thereby convert the oxidized fiber to a carbon fiber.
A process for producing a carbon fiber having high tensile strength which comprises oxidizing an organic polymeric fiber in an oxidizing atmosphere by intermittently contacting and removing said organic fiber on and from a heated body having a surface temperature from about 200.degree. to about 400.degree. C. wherein the contact time of said organic fiber on the heated body per single contact is less than about 1 second and the temperature of said oxidizing atmosphere is maintained lower [thn] than the surface temperature of said heated body, and then carbonizing the oxidized fiber in a non-oxidizing atmosphere at a temperature above about 800.degree. C.
A process for producing a carbonizable oxidized fiber which comprises oxidizing an organic polymeric fiber in an oxidizing atmosphere by intermittently contacting and removing said organic fiber on and from a heated body having a surface temperature from about 200.degree. to about 400.degree. C. wherein the contact time of said organic fiber on the heated body per single contact is less than about 1 second and the temperature of said oxidizing atmosphere is maintained lower than the surface temperature of said heated body.
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