# US 9,938,664 B2 · Method and arrangement for clarifying green liquor > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 9,938,664 B2 - Document ID: US9938664B2 - Status: Granted - Kind: B2 - Application number: 15/187,210 - Filed: 2016-06-20 - Published: 2017-02-23 - Granted: 2018-04-10 - Earliest claimed: 2009-04-02 - Assignees: Cleanflow AB - Applicants: Mikael Lindstrom; Christofer Lindgren; Lennart Borjeson; Lennart Kallen - Inventors: Mikael Lindstrom; Christofer Lindgren; Lennart Borjeson; Lennart Kallen - Web page: https://patentgrep.com/patent/US9938664B2 ## CPC - D21C 11/0078: {Treatment of green or white liquors with other means or other compounds than gases, e.g. in order to separate solid compounds such as sodium chloride and carbonate from these liquors; Further treatment of these compounds (fractionating of spent liquors D21C11/0042)} - B01D 61/147: {Microfiltration} - B01D 69/04: Tubular membranes - B01D 71/02: Inorganic material - B01D 2311/252: Recirculation of concentrate - B01D 2317/02: Elements in series - B01D 2325/02834: more than 0.1 and up to 1 µm - D21C: PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR - B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28) ## Abstract Green liquor clarification comprising filtering of a flowing suspension containing solids, wherein the suspension is brought into contact with a first filter unit (4), said 5 filter unit (4) comprising one or several filter elements (12) comprising one or several filter bodies (3) having filter channels (33) within the filter bodies (3) with a filtering layer (32), a part of the suspension is forced to pass through the filtering layer (32) from a first/inner surface (32A) to a second/outer surface (32B) of the filtering layer (32) forming a filtrate while the solids substantially remains in a residual part of the suspension forming a slurry and where the filtering layer (32) is made of a membrane material with pores, said pores having a pore size of 0.1-10 micrometer, more preferred 0.1-5 micrometer and most preferred 0.2-1.0 micrometer. ## Claims ### Claim 1 A method for clarifying green liquor comprising: providing an arrangement for green liquor clarification comprising: a filter unit comprising a green liquor inlet, a slurry outlet and a filtrate outlet, and being constructed to filter green liquor; a source of flowing green liquor comprising a suspension of solids connected to the green liquor inlet of the filter unit; a pump constructed to force the flowing green liquor into the green liquor inlet to provide a Reynolds Number between 10,000-45,000 and cause a turbulent flow within the filter unit; a recirculation conduit connecting the slurry outlet to the source of flowing green liquor and being constructed for recirculating at least a portion of a slurry from the filter unit back to the source of flowing green liquor; a recirculation valve constructed to control an amount of slurry being recirculated from the slurry outlet to the source of flowing green liquor, wherein said filter unit comprising one or several filter elements, comprising one or several filter bodies having filter channels within the filter bodies with a filtering layer, during use a part of the green liquor is forced to pass through the filtering layer from a first inner surface to a second outer surface of the filtering layer forming a filtrate while the solids substantially remain in a residual part of the green liquor forming the slurry, wherein the filtering layer comprises a membrane material having pores, and said pores having a pore size of 0.1-10 micrometer, wherein the filter unit is constructed such that during use the filtrate flow from the filter unit is less than 50% of the green liquor flow into the filter unit, and the Renolds Number can be controlled by controlling the flow of the slurry out of the filer unit to provide the turbulent flow and prevent build-up of a filter cake in the filtering unit; a mud filter constructed for dewatering the slurry during use and form a dry solid suitable for landfill; and a slurry conduit connecting the slurry outlet to the mud filter; using the pump to flow the flowing green liquor from the source of green liquor into the inlet of the filter unit inlet; forming the slurry in the filter unit; flowing the at least a portion of the slurry through the recirculation valve, the recirculation conduit, and the slurry outlet to the source of flowing green liquor to recirculate the at least a portion of the slurry back to the source of flowing green liquor; flowing at least a portion of the slurry through the slurry valve and slurry conduit to the mud filter; operating and using the pump and/or the recirculation valve to control and provide a Renolds Number between 10,000-45,000 and provide a turbulent flow and prevent build-up of a filter cake in the filtering unit, wherein the filter inlet and filter unit are constructed and operated so that the flow of green liquor through the filter unit is upstream against a direction of a gravitational force, and the filter channels have a converging cross-sectional area to maintain the Reynolds Number within an entire length of the filter channels and operating the filter and operating the arrangement to provide the Reynolds Number within the entire length of the filter channels. ### Claim 2 (depends on 1) The method according to claim 1, wherein the pores have a size of 0.2-1.0 micrometer. ### Claim 3 (depends on 1) The method according to claim 1, further comprising a slurry valve constructed to control a flow of slurry from the filter unit to the slurry conduit. ### Claim 4 (depends on 1) The method according to claim 1, operating and using the pump, the slurry valve, and/or the recirculation valve to control and provide a Renolds Number between 10,000-45,000 and provide a turbulent flow and prevent build-up of a filter cake in the filtering unit. ### Claim 5 (depends on 1) The method according to claim 1, further comprising operating and using the pump, the recirculation valve and/or the slurry valve to control and provide a Reynolds Number between 12,000-17,000. ### Claim 6 (depends on 1) The method according to claim 1, wherein said membrane material is ceramic. ### Claim 7 (depends on 1) The method according to claim 1, wherein said source of green liquor is a cleaning unit for green liquor. ### Claim 8 (depends on 7) The method according to claim 7, wherein said filter unit is arranged as a first filtering step before final cleaning of the remaining slurry in the cleaning unit. ### Claim 9 (depends on 7) The method according to claim 7, wherein the filter unit is arranged to filter cleaned green liquor. ### Claim 10 (depends on 1) The method according to claim 1, wherein the filter unit is constructed and operated such that the filtrate flow from the filter unit is less than 40% of the green liquor flow into the filter unit. ### Claim 11 (depends on 1) The method according to claim 1, wherein the filter unit is constructed and operated such that the filtrate flow from the filter unit is less than 30% of the green liquor flow into the filter unit. ### Claim 12 (depends on 1) The method according to claim 1, wherein the filter unit is constructed and operated such that the filtrate flow from the filter unit is not less than 5% of the green liquor flow into the filter unit. ### Claim 13 (depends on 1) The method according to claim 1, further comprising a conduit connecting the filtrate outlet to a white liquor preparation and supply at least a portion of the filtrate to the white liquor preparation.