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US 9,868,682 B2Granted
Production of partially refined waste glycerol
AssigneeReg Life Sciences, LLC
InventorsMyong K. Ko, Fernando A. Sanchez-Riera, Simon Li, Perry Y. Liao
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Abstract
The disclosure relates to a novel glycerol purification process that produces partially refined waste glycerol for a variety of industrial applications. The disclosure encompasses a salt-containing partially refined glycerol composition that is suitable as a fermentation grade glycerol.
Claims8
A process of producing partially refined waste glycerol by refining crude glycerol containing organic impurities, said process comprising:
- subjecting crude glycerol to a hydrophobic solvent to produce a mixture of crude glycerol and hydrophobic solvent;
- separating the mixture of crude glycerol and hydrophobic solvent to produce a deoiled (DO) glycerol and a phase containing hydrophobic solvent and organic impurities;
- drying said DO glycerol to produce a deoiled and dewatered (DOW) glycerol;
- subjecting a polar solvent to said DOW glycerol to produce a mixture of polar solvent and DOW glycerol and precipitating a salt from the mixture of polar solvent and DOW glycerol;
- and separating the mixture of polar solvent and DOW glycerol into a light phase containing a deoiled, dewatered and desalted (DOWS) glycerol and the polar solvent and a heavy phase containing the salt, wherein said process further comprises:
- partially evaporating about 75 percent of said DOW glycerol as a glycerol distillate without salt;
- recovering a remaining portion of said DOW glycerol in an evaporation discharge bottom;
- and adding the polar solvent to said evaporation discharge bottom to precipitate salt and create a deoiled, dewatered and desalted (DOWS) glycerol.
5 more elements
Dependencies are inferred from the claim text.