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US 9,755,231 B2Granted
Method of preparing iron oxide nanoparticles
AssigneeLG Chem, Ltd.
InventorsMyung Ki Lee, Sung Bin Park, Sung Joong Kang, Wang Mo Jung
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Abstract
Provided are a method of preparing iron oxide nanoparticles, iron oxide nanoparticles prepared thereby, and an anode material including the iron oxide nanoparticles.
Claims2
A method of preparing oval shaped iron (III) oxide nanoparticles, the method comprising:
- preparing a ferric chloride (FeCl3) aqueous solution;
- preparing a sodium hydroxide (NaOH) aqueous solution;
- obtaining a mixed aqueous solution consisting of the ferric chloride (FeCl3) aqueous solution, the sodium hydroxide (NaOH) aqueous solution, and a sodium sulfate (Na2SO4) aqueous solution;
- reacting the mixed aqueous solution in an electric convection oven in a temperature range of 100° C. to 105° C. for 90 hours to 100 hours at atmospheric pressure to get a solid product;
- and
- cooling, washing, and drying the solid product to get a dried product,
- wherein a concentration of the FeCl3 aqueous solution is in a range of 2 M to 3 M,
- a concentration of the NaOH aqueous solution is in a range of 5 M to 6 M,
- a concentration of the Na2SO4 aqueous solution is in a range of 0.5 M to 1 M, and
- the dried product consists of iron (III) oxide.
7 more elements
Dependencies are inferred from the claim text.