# US 9,752,987 B1 · Hydride generation system

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- Number: US 9,752,987 B1
- Document ID: US9752987B1
- Status: Granted
- Kind: B1
- Application number: 14/635,887
- Filed: 2015-03-02
- Granted: 2017-09-05
- Earliest claimed: 2014-02-28
- Assignees: Elemental Scientific, Inc.
- Applicants: Elemental Scientific, Inc.
- Inventors: Daniel R. Wiederin; Austin Schultz
- Web page: https://patentgrep.com/patent/US9752987B1

## CPC

- H02P 25/188: {wherein the motor windings are switched from series to parallel or vice versa to control speed or torque}
- B63H 21/14: relating to internal-combustion engines {(of outboard type B63H20/00)}
- B63H 21/20: the vessels being powered by combinations of different types of propulsion units
- B63H 23/10: for transmitting drive from more than one propulsion power unit
- C01B 6/00: Hydrides of metals {including fully or partially hydrided metals, alloys or intermetallic compounds (use of some thereof for reversible sorption of hydrogen C01B3/0005, C01B3/508); Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH}; Monoborane or diborane; Addition complexes thereof (higher hydrides of boron, substituted hydrides of boron C01B35/00)
- C01B 6/06: Hydrides of aluminium, gallium, indium, thallium, germanium, tin, lead, arsenic, antimony, bismuth or polonium; Monoborane; Diborane; Addition complexes thereof
- C01B 6/10: Monoborane; Diborane; Addition complexes thereof
- G01N 21/714: {Sample nebulisers for flame burners or plasma burners (nebulizers per se B05B)}
- G01N 21/73: using plasma burners or torches
- H02K 3/28: Layout of windings or of connections between windings (windings for pole-changing H02K17/06, H02K17/14, H02K19/12, H02K19/32)
- H02K 7/183: {wherein the turbine is a wind turbine (adaptation of a wind turbine to an electric generator F03D9/25)}
- H02K 16/04: Machines with one rotor and two stators
- H02K 19/16: Synchronous generators
- H02K 21/024: {Radial air gap machines}
- H02P 31/00: Arrangements for regulating or controlling electric motors not provided for in groups H02P1/00 - H02P5/00, H02P7/00 or H02P21/00 - H02P29/00
- B63H 2021/202: {of hybrid electric type}
- B63H 2021/205: {the second power unit being of the internal combustion engine type, or the like, e.g. a Diesel engine}
- Y02T 70/5236: Renewable or hybrid-electric solutions
- Y10S 903/906: Motor or generator
- H02P: CONTROL OR REGULATION OF ELECTRIC MOTORS, ELECTRIC GENERATORS OR DYNAMO-ELECTRIC CONVERTERS; CONTROLLING TRANSFORMERS, REACTORS OR CHOKE COILS
- B63H: MARINE PROPULSION OR STEERING (propulsion of air-cushion vehicles B60V1/14; specially adapted for submarines, other than nuclear propulsion, B63G; specially adapted for torpedoes F42B19/00)
- C01B: NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; {METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C}
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- H02K: DYNAMO-ELECTRIC MACHINES (dynamo-electric relays H01H53/00; conversion of DC or AC input power into surge output power {H03K3/53})
- Y02T: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
- Y10S: TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

## Abstract

The present disclosure is directed to a system and a method for hydride generation. In some embodiments, the system includes an assembly for introducing hydride generation reagents into a mixing path or mixing container, where the assembly includes first chamber configured to contain a first hydride generation reagent and a second chamber configured to contain a second hydride generation reagent. A first plunger is configured to translate within the first chamber and cause a displacement of the first hydride generation reagent, and a second plunger is configured to translate within the second chamber and cause a displacement of the second hydride generation reagent. The assembly further includes base coupling the first plunger and the second plunger together.

## Claims

### Claim 1

A system, comprising:
a first chamber configured to contain a first hydride generation reagent;
a second chamber configured to contain a second hydride generation reagent;
a first plunger configured to translate within the first chamber and cause a displacement of the first hydride generation reagent;
a second plunger configured to translate within the second chamber and cause a displacement of the second hydride generation reagent; and
a base coupling the first plunger and the second plunger together, the base vertically movable relative to the first chamber and the second chamber.

### Claim 2 (depends on 1)

The system as recited in claim 1, wherein the first plunger and the second plunger are moveably coupled to the base.

### Claim 3 (depends on 2)

The system of claim 2, wherein the first plunger and the second plunger are moveably coupled to the base by at least one pin extending through at least a portion of the base.

### Claim 4 (depends on 1)

The system of claim 1, wherein the first chamber and the second chamber are rigidly connected with one another.

### Claim 5 (depends on 4)

The system of claim 4, wherein the first chamber and the second chamber are portions of a common structure.

### Claim 6 (depends on 4)

The system of claim 4, further comprising one or more mounting members rigidly connected to the first and second chambers, the one or more mounting members configured for affixing the first and second chambers to a rigid structure.

### Claim 7 (depends on 6)

The system of claim 6, further comprising:
an actuator coupled to the rigid structure or the base; and
a controller configured to cause the actuator to actuate the rigid structure or the base to dispense a selected amount of the first hydride generation reagent and a selected amount of the second hydride generation reagent.

### Claim 8 (depends on 1)

The system of claim 1, further comprising:
a third chamber configured to contain a carrier solution; and
a third plunger configured to translate within the third chamber and cause a displacement of the carrier solution, wherein the base further couples the third plunger with the first plunger and the second plunger together.

### Claim 9 (depends on 8)

The system of claim 8, wherein a cross-sectional area of the first chamber is different from a cross-sectional area of the second chamber, or a cross-sectional area of the first chamber is different from a cross-sectional area of the third chamber, or a cross-sectional area of the second chamber is different from a cross-sectional area of the third chamber.

### Claim 10 (depends on 8)

The system of claim 8, wherein the third plunger is coupled with the base, and the base and the third plunger together are movable relative to the third chamber.

### Claim 11 (depends on 1)

The system of claim 1, wherein the first chamber and the second chamber are sized appropriately to dispense the first hydride generation reagent and the second hydride generation reagent in a ratio suitable for forming a hydride when mixed with a sample.

### Claim 12 (depends on 1)

The system of claim 1, wherein the first plunger and the second plunger are configured respectively to displace fluid within the first chamber and the second chamber in a synchronized manner when the base, the first plunger, and the second plunger together are moved relative to the first chamber and the second chamber.
