# US 9,751,119 B2 · Composition, method and apparatus for soil remediation

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- Number: US 9,751,119 B2
- Document ID: US9751119B2
- Status: Granted
- Kind: B2
- Application number: 14/196,891
- Filed: 2014-03-04
- Published: 2015-09-10
- Granted: 2017-09-05
- Earliest claimed: 2013-03-04
- Applicants: Jose Rafael Hernandez; Antonio Ruben Camacho
- Inventors: Jose Rafael Hernandez; Antonio Ruben Camacho
- Web page: https://patentgrep.com/patent/US9751119B2

## CPC

- B09C 1/08: chemically
- B09C 1/02: Extraction using liquids, e.g. washing, leaching {, flotation}
- B09C 1/025: {using an oil as solvent or extracting agent}
- B09C: RECLAMATION OF CONTAMINATED SOIL (gatherers for removing stone or the like from the soil A01B43/00; sterilising soil by steam A01G11/00; removing undesirable matter, e.g. rubbish, from the land E01H15/00)

## Abstract

The disclosure describes a composition, process and apparatus for soil remediation on site using an encapsulating agent to separate contaminants from soil. The contaminated soil is saturated with the encapsulating agent, creating an immediate reaction causing the contaminants to dissociate from the soil in favor of association with the encapsulating agent. The encapsulating agent attracts and associates with the contaminants but do not dissolve them, resulting in a clearly-defined heterogeneous mixture with at least three phases, wherein said phases include contaminants at the top of the mixture, encapsulation agent at the middle and cleansed soil at the bottom of the mixture.

## Claims

### Claim 1

A method for treatment of contaminated soil comprising:
a site with contaminated soil;
an encapsulating agent;
an encapsulating agent tank at least a first chamber and a second chamber,
wherein said encapsulating agent tank is filled with said encapsulating agent; and
a soil remediation process, wherein said remediation process comprises the steps of:
a) removing contaminated soil from site;
b) mixing said contaminated soil with said encapsulating agent to create an admixture, wherein said admixture comprises at least a first phase and a second phase, wherein said first phase comprises at least cleansed soil, and said second phase comprises at least one contaminant and the encapsulating agent;
c) agitating the admixture;
d) removing the first phase from said second phase;
e) redirecting said second phase to the first chamber of the encapsulating agent tank;
f) saturating said second phase with the encapsulating agent;
g) removing from said second phase the contaminant;
h) redirecting the encapsulating agent from the bottom of said first chamber to the second chamber through an inlet between the first chamber and the second chamber; and
i) recycling back the encapsulating agent in the soil remediation process.

### Claim 2 (depends on 1)

The method for treatment of contaminated soil as in claim 1, wherein the encapsulating agent comprises: i) an anionic surfactant, ii) an alcohol; iii) a non-ionic surfactant; iv) pine oil; and v) water.

### Claim 3 (depends on 1)

The method for treatment of contaminated soil as in claim 1, wherein the encapsulating agent comprises: i) 0.8-6% wt. of an anionic surfactant, ii) 0.8-6% wt. of an alcohol; iii) 0.4-3% wt. of a non-ionic surfactant; iv) 0.8-6% wt. of pine oil; and v) 90-97% wt. of water.

### Claim 4 (depends on 1)

The method for treatment of contaminated soil as in claim 1 wherein the encapsulating agent comprises: i) 0.8-6% wt. of sodium lauryl sulfate; ii) 0.8-6% wt. of isopropyl alcohol; iii) 0.4-3% wt. of ethoxylated alcohol; iv) 0.8-6% wt. of pine oil; and v) 90-97% wt. of water.

### Claim 5 (depends on 1)

The method for treatment of contaminated soil as in claim 1, wherein the contaminated soil is mixed and saturated with the encapsulating agent in at least a 3:1 ratio.

### Claim 6 (depends on 1)

The method for treatment of contaminated soil as in claim 1, wherein said encapsulating agent is water-soluble and biodegradable.

### Claim 7 (depends on 1)

The method for treatment of contaminated soil as in claim 1, wherein the step of removing the first phase from the second phase comprises a shaker.

### Claim 8 (depends on 7)

The method for treatment of contaminated soil as in claim 7, wherein said shaker comprises a screen having a mesh size, said mesh size is small enough to avoid the first phase to pass through said mesh.

### Claim 9 (depends on 1)

The method for treatment of contaminated soil as in claim 1, wherein the second phase comprises at least a first density and a second density, wherein the first density is the contaminant and the second density is the encapsulating agent.

### Claim 10 (depends on 9)

The method for treatment of contaminated soil as in claim 9, wherein the step for removing the contaminants from the second phase comprises at least a first pump.