# US 9,751,064 B2 · Vortex chamber device, and method for treating powder particles or a powder particles precursor > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 9,751,064 B2 - Document ID: US9751064B2 - Status: Granted - Kind: B2 - Application number: 14/438,040 - Filed: 2013-10-25 - Published: 2015-10-01 - Granted: 2017-09-05 - Earliest claimed: 2012-10-26 - Assignees: Friesland Brands B.V.; Université Catholique De Louvain - Applicants: Friesland Brands B.V.; Université Catholique De Louvain - Inventors: Juray De Wilde; Philippe Edouard Jean Eliaers; Albert Thijs Poortinga - Web page: https://patentgrep.com/patent/US9751064B2 ## CPC - B01J 2/16: by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain - B01J 2/003: {followed by coating of the granules (to prevent the granules sticking together B01J2/30)} - B01J 8/14: moving in free vortex flow apparatus - B01J 8/1818: {Feeding of the fluidising gas (B01J8/44 takes precedence)} - B01J 8/1827: {the fluidising gas being a reactant} - B01J 8/36: with fluidised bed through which there is an essentially horizontal flow of particles - B01J 8/386: {internally, i.e. the particles rotate within the vessel} - B05C 19/02: using fluidised-bed techniques (fluidised-bed technique in general B01J8/24) - B05D 1/12: Applying particulate materials (B05D1/06, B05D1/10 take precedence) - B05D 1/24: Applying particulate materials - B01J 2208/00902: Nozzle-type feeding elements - B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS - B05C: APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL (spraying apparatus, atomising apparatus, nozzles B05B; plant for applying liquids or other fluent materials to objects by electrostatic spraying B05B5/08) - B05D: PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL (conveying articles or workpieces through baths of liquid B65G, e.g. B65G49/02) ## Abstract A vortex chamber device comprising: a reactor comprising at least one chamber having a substantially circular cross-section; a device for feeding at least one fluid that is gaseous or liquid into the chamber; a device for removing said one or more fluids from the chamber; a device for feeding powder particles or a powder particles precursor to said chamber; wherein said fluid removing device comprises at least one discharge opening for removing said at least one fluid from the chamber. The invention also provides a method for treating powder particles or a powder particles precursor. ## Claims ### Claim 1 A vortex chamber device comprising: a reactor comprising at least one chamber having a substantially circular cross-section; a device for feeding at least one fluid that is gaseous or liquid into the chamber; a device for removing said one or more fluids from the chamber; a device for feeding powder particles or a powder particles precursor to said chamber; wherein said fluid removing device comprises at least one discharge opening for removing said at least one fluid from the chamber; wherein said fluid feeding device comprises fluid injectors distributed around a chamber wall for injecting said at least one fluid along said wall, for transferring momentum to said powder particles or the powder particles precursor to enable a rotational movement whereby a centrifugal force thrusts the particles or precursor toward said wall through said injected fluid; said powder particles or the powder particles precursor thereby forming a rotating fluidized bed which rotates around and at a certain distance from said fluid discharge opening while sliding along said chamber wall and while being at least partially supported by said at least one fluid which passes through said fluidized bed before being removed via said discharge opening; wherein said fluid feeding device comprises more than 11 primary fluid injectors, with each of the fluid injectors including a fluid injection slit having a slit width that is smaller than 1 mm. ### Claim 2 (depends on 1) The vortex chamber device according to claim 1, wherein said fluid feeding device comprises at least 30 fluid injectors. ### Claim 3 (depends on 1) The vortex chamber device according to claim 1, wherein said fluid feeding device comprises at least 50 to 70 fluid injectors. ### Claim 4 (depends on 1) The vortex chamber device according to claim 1, wherein each of the fluid injectors has a slit width in the range of about 0.1-0.2 mm. ### Claim 5 (depends on 1) The vortex chamber device according to claim 1, including a device for removing powder particles via a side of said chamber that is remote from said fluid injectors. ### Claim 6 (depends on 1) The vortex chamber device according to claim 1, the chamber including a first section that includes said primary fluid injectors, and a second section adjoining the first section, the second chamber section including a plurality of secondary fluid injectors for feeding a fluid into the chamber that differs from fluid that is injected by the primary fluid injectors. ### Claim 7 (depends on 6) The vortex chamber device of claim 6, including a partition for partly separating the first and second chamber sections from each other. ### Claim 8 (depends on 1) A device according to claim 1, including a sprayer, for feeding liquid into the chamber. ### Claim 9 (depends on 1) A method for treating powder particles or a powder particles precursor, utilizing a vortex chamber device according to claim 1, the method including the steps of: injecting at least one fluid along a wall of a chamber having a substantially circular cross-section; removing said one or more fluids from the chamber via a fluid discharge opening; feeding powder particles or a powder particles precursor to said chamber, wherein the injected fluid transfers momentum to said powder particles or the powder particles precursor to enable a rotational movement whereby a centrifugal force thrusts the particles or the precursor toward said wall through said injected fluid, wherein the powder particles or the powder particles precursor form a rotating fluidized bed which rotates around and at a certain distance from said fluid discharge opening while sliding along said wall and while being at least partially supported by said at least one fluid which passes through said fluidized bed before being removed via said discharge opening; wherein said fluid is injected via more than 11 primary fluid injectors, each generating a fluid layer having a layer thickness at the respective fluid injector that is smaller than 1 mm, wherein more than 30 primary fluid injectors are used, generating fluid layers having layer thicknesses at the respective fluid injector smaller than 0.5 mm. ### Claim 10 (depends on 9) A method according to claim 9, including feeding a liquid powder particles precursor to the chamber, and substantially drying the precursor in the chamber for generating powder particles. ### Claim 11 (depends on 9) A method according to claim 9, including spraying a fluid powder particles precursor into the chamber, the spraying particularly including atomizing the fluid, the fluid particularly being a liquid. ### Claim 12 (depends on 9) A method according to claim 9, including feeding a coating substance to the chamber to coat the powder particles. ### Claim 13 (depends on 9) A method according to claim 9, wherein the powder particles have a density that is lower than 2500 kg/m3. ### Claim 14 (depends on 9) A method according to claim 9, wherein the powder particles have a density that is lower than 1000 kg/m3. ### Claim 15 (depends on 9) A method according to claim 9, wherein the powder particles have a size density (D50) that is smaller than 500 micron.