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US 9,540,279 B2Granted
Method of producing glass-ceramic
AssigneeCorning Incorporated
InventorCarlos Eduardo Folgar
Life of this patent
Estimating the term…
Abstract
A method of producing glass-ceramic includes providing a glass made from a glass composition comprising LiO2, Al2O3, SiO2, and at least one nucleating agent. The glass is disposed in a microwave processing chamber. Microwaves are then selectively delivered into the microwave processing chamber at varying frequencies to induce different distributions of microwave fields in the glass. The glass is nucleated and crystallized while under the influence of the induced microwave fields.
Claims9
A method of producing glass-ceramic, comprising:
- providing a glass made from a glass composition comprising LiO2, Al2O3, SiO2, and at least one nucleating agent;
- disposing the glass in a microwave processing chamber;
- selectively delivering microwaves into the microwave processing chamber at varying frequencies in a range from 5.4 GHz to 7.0 GHz to induce different distributions of microwave fields in the glass;
- heating the glass to a nucleation temperature under the influence of the induced microwave fields;
- maintaining the glass at the nucleation temperature under the influence of the induced microwave fields for a time period during which crystal nuclei develop in the glass;
- heating the glass to a crystallization temperature under the influence of the induced microwave fields;
- maintaining the glass at the crystallization temperature under the influence of the induced microwave fields for a time period during which at least one crystalline phase grows in the glass, thereby forming a glass-ceramic;
- and
- cooling the glass-ceramic from the crystallization temperature to room temperature, the cooling comprising an initial phase in which microwaves are applied to the glass-ceramic, wherein a temperature of the glass-ceramic drops by 5% to 20% of the crystallization temperature during the initial phase of the cooling.
6 more elements
Dependencies are inferred from the claim text.