# US 9,518,944 B2 · Temperature-controlled bath

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- Number: US 9,518,944 B2
- Document ID: US9518944B2
- Status: Granted
- Kind: B2
- Application number: 14/295,781
- Filed: 2014-06-04
- Published: 2015-01-01
- Granted: 2016-12-13
- Earliest claimed: 2013-06-27
- Assignees: Mitutoyo Corporation
- Applicants: Mitutoyo Corporation
- Inventors: Yuichiro Yokoyama; Takeshi Hagino
- Web page: https://patentgrep.com/patent/US9518944B2

## CPC

- G01N 25/16: by investigating thermal coefficient of expansion
- G01N 1/44: Sample treatment involving radiation, e.g. heat
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

A temperature-controlled bath capable of swiftly changing the temperature of a sample to a target temperature and maintaining the temperature of the sample at a fixed temperature after the temperature change is provided. A temperature-controlled bath includes a temperature changing means, a temperature-controlled chamber, a sample holding chamber, and connection cut-off means. The temperature changing means is disposed in the temperature-controlled chamber, and the temperature of the temperature-controlled chamber is adjusted by the temperature changing means. The sample holding chamber is separated from the temperature-controlled chamber by a thermally conducive wall, and contains a sample therein. The connection cut-off means change a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state.

## Claims

### Claim 1

A temperature-controlled bath comprising:
temperature changing means for heating or cooling a gas so that the temperature of the gas is adjusted to a set temperature;
a temperature-controlled chamber whose temperature is adjusted by the temperature changing means, the temperature changing means being disposed in the temperature-controlled chamber;
a sample holding chamber containing a sample therein, the sample holding chamber being separated from the temperature-controlled chamber by a thermally conductive wall;
and connection cut-off means for changing a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state.

### Claim 2 (depends on 1)

The temperature-controlled bath according to claim 1, further comprising first blower means for sending a gas whose temperature is adjusted by the temperature changing means mainly into the temperature-controlled chamber.

### Claim 3 (depends on 1)

The temperature-controlled bath according to claim 1, further comprising
an air hole that serves as an inlet/outlet of the gas between the temperature-controlled chamber and the sample holding chamber;
second blower means for sending the gas in the temperature-controlled chamber into the sample holding chamber through the air hole; and
third blower means for sending out the gas in the sample holding chamber toward the temperature-controlled chamber through the air hole.

### Claim 4 (depends on 1)

The temperature-controlled bath according to claim 1, wherein the thermally conductive wall comprises at least one of a radiator plate protruding toward the temperature-controlled chamber and a radiator plate protruding toward the sample holding chamber.

### Claim 5 (depends on 1)

The temperature-controlled bath according to claim 1, wherein the sample holding chamber comprises a probe inserting hole for inserting a probe into the sample holding chamber, the probe inserting hole being able to be opened and closed.

### Claim 6 (depends on 1)

The temperature-controlled bath according to claim 1, wherein the sample holding chamber comprises an optically transparent window for enabling optical measurement of the sample.

### Claim 7 (depends on 1)

The temperature-controlled bath according to claim 1, wherein
the connection cut-off means is an open/close shutter that opens/closes by rotating a plate member, and
the plate member is an air-permeable plate member capable of letting a gas pass through the plate member.

### Claim 8

A linear expansion coefficient measuring device comprising:
a temperature-controlled bath;
measurement means for measuring a length of the sample at different temperatures; and calculation means for calculating a coefficient of linear expansion of the sample based on the length of the sample at each temperature, wherein
the temperature-controlled bath comprises:
temperature changing means for heating or cooling a gas so that the temperature of the gas is adjusted to a set temperature;
a temperature-controlled chamber whose temperature is adjusted by the temperature changing means, the temperature changing means being disposed in the temperature-controlled chamber;
a sample holding chamber containing a sample therein, the sample holding chamber being separated from the temperature-controlled chamber by a thermally conductive wall; and
connection cut-off means for changing a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state.

### Claim 9

A temperature-controlled bath comprising:
a temperature changing unit that heats or cools a gas so that the temperature of the gas is adjusted to a set temperature;
a temperature-controlled chamber whose temperature is adjusted by the temperature changing unit, the temperature changing unit being disposed in the temperature-controlled chamber;
a sample holding chamber containing a sample therein, the sample holding chamber being separated from the temperature-controlled chamber by a thermally conductive wall; and
a connection cut-off unit that changes a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state.

### Claim 10 (depends on 9)

The temperature-controlled bath according to claim 9, further comprising a first blower unit that sends a gas whose temperature is adjusted by the temperature changing unit mainly into the temperature-controlled chamber.

### Claim 11 (depends on 9)

The temperature-controlled bath according to claim 9, further comprising
an air hole that serves as an inlet/outlet of the gas between the temperature-controlled chamber and the sample holding chamber;
a second blower unit that sends the gas in the temperature-controlled chamber into the sample holding chamber through the air hole; and
a third blower unit that sends out the gas in the sample holding chamber toward the temperature-controlled chamber through the air hole.

### Claim 12 (depends on 9)

The temperature-controlled bath according to claim 9, wherein
the connection cut-off unit is an open/close shutter that opens/closes by rotating a plate member, and
the plate member is an air-permeable plate member capable of letting a gas pass through the plate member.
