# US 9,517,593 B2 · Apparatus and process for producing porous devices

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- Number: US 9,517,593 B2
- Document ID: US9517593B2
- Status: Granted
- Kind: B2
- Application number: 14/985,206
- Filed: 2015-12-30
- Published: 2016-04-21
- Granted: 2016-12-13
- Earliest claimed: 2014-06-26
- Assignees: Vertera, Inc.
- Applicants: Vertera, Inc.
- Inventors: Wei-Hsiang Chang; Stephen Lee Laffoon; Christopher S. D. Lee; David Lee Safranski
- Web page: https://patentgrep.com/patent/US9517593B2

## CPC

- B29C 67/202: {comprising elimination of a solid or a liquid ingredient}
- B29K 2071/00: Use of polyethers {, e.g. PEEK, i.e. polyether-etherketone or PEK, i.e. polyetherketone or derivatives thereof}, as moulding material
- B29K 2105/12: of short lengths, e.g. chopped filaments, staple fibres or bristles
- B29K 2105/16: Fillers
- B29K 2105/256: {Sheets, plates, blanks or films}
- B29K 2507/04: Carbon
- B29C: SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING (making preforms B29B11/00; making laminated products by combining previously unconnected layers which become one product whose layers will remain together B32B37/00 - B32B41/00)
- B29K: INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR {MOULDS, } REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS

## Abstract

In general, in various embodiments, the present disclosure is directed systems and methods for producing a porous surface from a solid piece of polymer. In particular, the present disclosure is directed to systems that include a track assembly, mold assembly, press assembly, and methods for using the same for producing a porous surface from a solid piece of polymer. In some embodiments, the present systems and methods are directed to processing a polymer at a temperature below a melting point of the polymer to produce a solid piece of polymer with an integrated a porous surface.

## Claims

### Claim 1

A method for processing material, the method comprising:
providing a piece of polymer for processing;
pressing a surface of the piece of polymer against a layer of porogen via a static weight;
while the piece of polymer is pressed against the layer of porogen, subjecting the piece of polymer to at least one heat zone along a track assembly, wherein the at least one heat zone heats the material to a particular temperature for a particular time;
further pressing the piece of polymer against the layer of porogen via a press assembly such that at least a portion of the layer of porogen is displaced through a surface of the piece of polymer to create a matrix layer of porogen and the polymer; and
removing the porogen from the matrix layer of the polymer thereby creating a porous layer of the polymer, wherein:
the at least one heat zone is a first zone and a second zone along the track assembly; and
the first zone and the second zone heat the piece of polymer to substantially the same temperature.

### Claim 2

A method for processing material, the method comprising:
providing a piece of polymer for processing;
pressing a surface of the piece of polymer against a layer of porogen via a static weight;
while the piece of polymer is pressed against the layer of porogen, subjecting the piece of polymer to at least one heat zone along a track assembly, wherein the at least one heat zone heats the material to a particular temperature for a particular time;
further pressing the piece of polymer against the layer of porogen via a press assembly such that at least a portion of the layer of porogen is displaced through a surface of the piece of polymer to create a matrix layer of porogen and the polymer; and
removing the porogen from the matrix layer of the polymer thereby creating a porous layer of the polymer, wherein the at least one zone is a plurality of zones and each of the plurality of zones each heats the piece of polymer to a different temperature.

### Claim 3 (depends on 2)

The method of claim 2, wherein:
the at least one zone is a first zone, a second zone, and a third zone; and
each of the first zone, second zone, and third zone each heats the piece of polymer to a different temperature.

### Claim 4

A method for processing material, the method comprising:
providing a piece of polymer for processing;
pressing a surface of the piece of polymer against a layer of porogen via a static weight;
while the piece of polymer is pressed against the layer of porogen, subjecting the piece of polymer to at least one heat zone along a track assembly, wherein the at least one heat zone heats the material to a particular temperature for a particular time;
further pressing the piece of polymer against the layer of porogen via a press assembly such that at least a portion of the layer of porogen is displaced through a surface of the piece of polymer to create a matrix layer of porogen and the polymer; and
removing the porogen from the matrix layer of the polymer thereby creating a porous layer of the polymer, wherein:
the piece of polymer is a piece of thermoplastic; and
the piece of polymer is at least 50% PEEK by weight.

### Claim 5

A method comprising:
loading a solid body of material and porogen into a mold;
heating, via a heating element located along a processing path, a surface of the solid body of material to a processing temperature that is below a melting temperature of the material by a melting temperature differential;
increasing heat from the processing temperature while applying a constant pressure to the solid body of material for displacing the porogen through the surface by a defined distance, creating, thereby, a matrix layer including the material and the porogen in the solid body of material, the matrix layer being integrally connected with the solid body of material;
maintaining throughout the heating and displacing steps, the constant pressure on the solid body of material;
applying an increased pressure above the constant pressure to the solid body of material via a press assembly while the heat is applied to the surface of the solid body of material, wherein:
the press assembly includes a load cell for measuring an amount of pressure applied to the solid body of material, wherein the amount of pressure is the increased pressure;
the solid body of a material has an initial height;
the porogen is arranged in a layer within the mold at a particular depth; and
the solid body of material rests upon the layer of porogen such that the solid body of material and the porogen layer have a combined second height;
lowering a ram of the press assembly from a first position to a second position, wherein the second position corresponds to the initial height as measured from a bottom of the mold, thereby exerting the increased pressure on the solid body of material;
raising the ram of the press assembly from the second position to the first position upon the load cell determining that the press assembly is applying substantially zero pressure to the solid body of material at the second position;
cooling the solid body of material once the porogen is displaced through the surface by a defined distance; and
unloading the solid body of material from the mold and removing the porogen to create an integrally connected porous layer in the solid body of material, wherein the constant pressure is applied to the solid body of material via a static weight.