# US 9,517,443 B2 · Device for polymerizing lactams in molds > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 9,517,443 B2 - Document ID: US9517443B2 - Status: Granted - Kind: B2 - Application number: 14/104,740 - Filed: 2013-12-12 - Published: 2014-06-26 - Granted: 2016-12-13 - Earliest claimed: 2012-12-13 - Assignees: Fundacion Tecnalia Research & Innovation - Applicants: Fundacion Tecnalia Research & Innovation - Inventors: Sonia Garcia Arrieta; Unai Morales Diez; Cristina Elizetxea Ezeiza; M Amaia De La Calle Lizarazu; Jose Ignacio Hernandez Vicente; Pablo Casado Francisco; Mikel Liceaga Ontoria - Web page: https://patentgrep.com/patent/US9517443B2 ## CPC - B01J 4/02: for feeding measured {, i.e. prescribed} quantities of reagents - B29B 7/7457: {Mixing heads without moving stirrer (B29B7/7438, B29B7/76 take precedence)} - B29C 67/246: {Moulding high reactive monomers or prepolymers, e.g. by reaction injection moulding [RIM], liquid injection moulding [LIM] (casting monomers B29C39/006, mixing construction B29B7/74)} - B29K 2077/00: Use of {PA, i.e.} polyamides, e.g. polyesteramides {or derivatives thereof}, as moulding material - B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS - B29B: PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS - B29C: SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING (making preforms B29B11/00; making laminated products by combining previously unconnected layers which become one product whose layers will remain together B32B37/00 - B32B41/00) - B29K: INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR {MOULDS, } REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS ## Abstract A device for polymerizing lactams in molds, comprising: a reservoir for storing lactam, wherein said reservoir is kept at a temperature which varies in the range of 135-150° C. for melting the lactam and keeping it in melted state; lactam feeding means comprising dosing pipes for feeding the lactam from the reservoir, first dosing means for feeding an initiator; second dosing means for feeding an activator; a mixing head configured to receive the lactam, the initiator and the activator from respectively said lactam feeding means, said first dosing means and said second dosing means. The initiator and activator are liquid, and the cited reservoir and lactam feeding means are located within a heater configured to maintain the temperature of the lactam at a substantially constant value until it reaches the mixing head. ## Claims ### Claim 1 A device for polymerizing lactams in molds, comprising: a reservoir for storing lactam, wherein said reservoir is kept at a temperature which varies in the range of 135-150° C. for melting the lactam and keeping it in melted state; lactam feeding means comprising dosing pipes for feeding the lactam from the reservoir, first dosing means for feeding an initiator; second dosing means for feeding an activator; a mixing head configured to receive the lactam, the initiator and the activator from respectively said lactam feeding means, said first dosing means and said second dosing means, the mixing head having three independent inlets for independently receiving the lactam, the initiator and the activator, to allow said lactam, initiator and activator respectively flow within the mixing head without mixing each other until the output of the mixing head is reached; and a mixing pipe located at the output of said mixing head and configured to put the lactam, initiator and activator in contact for the first time, in such a way that they are mixed up; wherein said initiator and activator are liquid, and the cited reservoir and lactam feeding means are located within a heater configured to maintain the temperature of the lactam at a substantially constant value until it reaches the mixing head, wherein the lactam feeding means further comprises a pump configured to pump the lactam from the reservoir and to dose it towards the mixing head, the pump being located within the heater, the device further comprising an engine for controlling the dosing of the pump, the engine being outside said heater and joined to the pump by means of a shaft passing through a wall of said heater. ### Claim 2 (depends on 1) The device of claim 1, wherein the lactam feeding means further comprises a pressure meter configured to stop the pump in the event of overpressure, said pressure meter being located inside said heater, thus maintaining the temperature of said pressure meter at a substantially constant value. ### Claim 3 (depends on 1) The device of claim 1, wherein the lactam feeding means further comprises a relief valve configured to be mechanically activated for clearing the lactam in the event of exceeding a maximum working pressure, said relief valve being located within said heater, thus maintaining the temperature of said relief valve at a substantially constant value. ### Claim 4 (depends on 1) The device of claim 1, wherein the lactam feeding means further comprises a three-ways valve located between the reservoir and the pump, for enabling the communication of the material flow from the reservoir to the pump, or from the reservoir to a drainpipe for clearing the reservoir, said three-ways valve being located within said heater, thus maintaining the temperature of said three-ways valve at a substantially constant value. ### Claim 5 (depends on 1) The device of claim 1, further comprising an electro valve configured to open when the pump is working and to close when the pump stops, preventing dripping, once the dosing of the lactam is completed. ### Claim 6 (depends on 1) The device of claim 1, wherein the mixing head comprises a radial inlet for the lactam, a first inlet for the initiator and a second inlet for the activator, the first inlet being connected to a first pipe and the second inlet to a second pipe, so that the lactam flow enters the mixing head perpendicular to the output shaft while the initiator and activator enter in parallel, in such a way that the initiator and activator come out by the central part of the mixing head while the lactam flow does it by the perimeter part. ### Claim 7 (depends on 6) The device of claim 6, wherein the first dosing means for feeding the initiator comprises a syringe driver joined to the first inlet of the mixing head and the second dosing means for feeding the activator comprise a syringe driver joined to the second inlet of the mixing head. ### Claim 8 (depends on 1) The device of claim 1, wherein said mixing head is tempered by means of flat resistances, in order to prevent solidification of the lactam and keep the temperature of the mix under control. ### Claim 9 (depends on 1) The device of claim 1, wherein the mixing pipe is a static mixer. ### Claim 10 (depends on 1) The device of claim 1, wherein in use, the temperature inside the heater is between 100° C. and 115° C. ### Claim 11 (depends on 1) The device of claim 1, further comprising an electric resistor surrounding the reservoir configured to increase the temperature of the lactam inside the reservoir so that the lactam reaches a temperature between 135° C. and 150° C.