A hydrofluorination process carried-out utilizing a fluidized bed hydrofluorination reactor unit including a primary fluidized bed hydrofluorination reactor fluidly interconnected with a secondary fluidized bed hydrofluorination reactor, the primary fluidized bed hydrofluorination reactor including a cyclonic plenum assembly, the process comprising:
- directing a partially-reacted gas stream withdrawn from the secondary fluidized bed hydrofluorination into the cyclonic plenum assembly through a gas/solids inlet pipe tangentially disposed with respect to an annular sidewall of the cyclonic plenum assembly to induce vortex flow within the cyclonic plenum assembly and promote the cyclonic separation of entrained solids from the partially-reacted gas stream;
- and
- removing the entrained solids separated from the partially-reacted gas stream through a solids drain pipe included within the cyclonic plenum assembly.