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US 9,458,083 B2Granted
Method for hydrolysing acetone cyanohydrin
AssigneeEvonik Roehm GmbH
InventorsArndt Selbach, Lorenza Sartorelli, Andreas Perl, Joachim Deinken, Stefanie Sohnemann, Norbert Mnich, Matthias Groemping, Udo Gropp, Thomas Mertz
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Abstract
The present invention relates to a process for hydrolysis of acetone cyanohydrin (ACH) by means of sulphuric acid within the ACH sulpho process for preparation of methacrylic acid (MAA) or methyl methacrylate (MMA).
Claims7
A process for hydrolysis of acetocyanohydrin, the process comprising:
- preparing methyl methacrylate in a loop reactor by using sulphuric acid as a precursor,
- wherein
- at least one heat exchanger present in the loop reactor is equipped with turbulators,
- at least one reaction component is fed into the loop reactor via a metering ring, which is installed externally and immediately upstream of a pump with a pump housing in the loop reactor,
- the at least one heat exchanger equipped with turbulators is positioned downstream of a metered addition of sulphuric acid and of acetocyanohydrin in flow direction, and
- the turbulators are turbulators with 100-1200 turns/m.
3 more elements
Dependencies are inferred from the claim text.