# US 9,435,724 B2 · Test method and fixture for obtaining material properties under biaxial loading > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 9,435,724 B2 - Document ID: US9435724B2 - Status: Granted - Kind: B2 - Application number: 14/306,666 - Filed: 2014-06-17 - Published: 2015-12-17 - Granted: 2016-09-06 - Earliest claimed: 2014-06-17 - Assignees: The Boeing Company - Applicants: The Boeing Company - Inventors: Russel J. Sanui; William P. Keith; Michael L. Hand - Web page: https://patentgrep.com/patent/US9435724B2 ## CPC - G01N 3/08: by applying steady tensile or compressive forces (G01N3/28 takes precedence) - G01N 2203/0019: Compressive - G01N 2203/0057: using stresses due to heating, e.g. conductive heating, radiative heating - G01N 2203/0067: Fracture or rupture - G01N 2203/0274: Tubular or ring-shaped specimens - G01N 2203/0282: Two dimensional, e.g. tapes, webs, sheets, strips, disks or membranes - G01N 2203/0658: using acoustic or ultrasonic detectors - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) ## Abstract A test method and corresponding fixture design are provided which enable loading a circular test coupon (made, e.g., of ceramic matrix composite material) to failure under biaxial loading conditions while recording strain and temperature. Biaxial loading requires approximately equal loads to be applied in two directions concurrently. The disclosed method uses liquid coolant (e.g., liquid nitrogen) to cool a ring made of metal alloy (e.g., aluminum alloy) that is disposed radially outward from and surrounds the outer edge of the test coupon. The cooled metal alloy ring contracts and compresses the test coupon until failure occurs. ## Claims ### Claim 1 A method for loading a circular test coupon, comprising: (a) placing a coolant ring made of metal alloy so that an inner circumferential portion of the coolant ring is disposed radially outward from and surrounding an outer circumferential portion of the test coupon, which coolant ring has a channel; and (b) initiating a flow through the channel of liquid coolant that has a temperature less than the temperature of the coolant ring, wherein the inner diameter of the coolant ring and the outer diameter of the test coupon are selected so that the inner circumferential portion of the coolant ring will exert radially inwardly directed compressive forces on the outer circumferential portion of the test coupon as the coolant ring is cooled by the liquid coolant. ### Claim 2 (depends on 1) The method as recited in claim 1, wherein the metal alloy is an aluminum alloy. ### Claim 3 (depends on 1) The method as recited in claim 1, wherein the test coupon is made of ceramic matrix composite material. ### Claim 4 (depends on 1) The method as recited in claim 1, wherein the test coupon has a hole in a center thereof. ### Claim 5 (depends on 1) The method as recited in claim 1, wherein the liquid coolant is liquid nitrogen. ### Claim 6 (depends on 1) The method as recited in claim 1, further comprising the following step performed prior to step (b): restraining the outer circumferential portion of the test coupon from bending relative to an inner circumferential portion of the test coupon. ### Claim 7 (depends on 1) The method as recited in claim 1, further comprising the following step performed prior to step (a): thermally coupling an inner circumferential portion of the test coupon to a heat sink. ### Claim 8 A test assembly comprising: a circular test coupon having a hole in a center and an outer circumference, said test coupon comprising an inner circumferential portion adjacent said hole and an outer circumferential portion adjacent said outer circumference; first and second reinforcing rings respectively adhered to respective surfaces of said outer circumferential portion of said test coupon; a coolant ring made of metal alloy and having an inner circumferential portion disposed radially outward from and surrounding said outer circumferential portion of said test coupon, said coolant ring comprising a first channel; and first and second centering rings coupled to said coolant ring, said first centering ring comprising a first annular projection in contact with said first reinforcing ring, and said second centering ring comprising a second annular projection in contact with said second reinforcing ring. ### Claim 9 (depends on 8) The test assembly as recited in claim 8, wherein said coolant ring has multiple inlets and outlets for the liquid coolant to evenly distribute cooling around said coolant ring. ### Claim 10 (depends on 8) The test assembly as recited in claim 8, wherein said coolant ring further comprises a first inlet and a first outlet in fluid communication with said first channel, a second channel, and a second inlet and a second outlet in fluid communication with said second channel. ### Claim 11 (depends on 8) The test assembly as recited in claim 8, wherein the metal alloy is an aluminum alloy. ### Claim 12 (depends on 8) The test assembly as recited in claim 8, wherein said test coupon is made of ceramic matrix composite material. ### Claim 13 (depends on 8) The test assembly as recited in claim 8, wherein said coolant ring comprises a base and a top coupled to each other by a plurality of fasteners. ### Claim 14 (depends on 8) The test assembly as recited in claim 8, further comprising first and second heat sink disks which are thermally coupled to respective surfaces of said inner circumferential portion of said test coupon. ### Claim 15 (depends on 14) The test assembly as recited in claim 14, wherein the test coupon has a hole in a center thereof, further comprising: a stud that passes through said hole; and a plurality of nuts that are coupled to said stud, wherein said first and second heat sink disks are coupled to said studs by said nuts. ### Claim 16 A test system comprising: a coolant ring made of metal alloy and comprising a central opening and a channel surrounding said central opening; first and second centering rings coupled to said coolant ring, said first centering ring comprising a first annular projection which projects into said central opening of said coolant ring, and said second centering ring comprising a second annular projection which projects into said central opening of said coolant ring, said first and second annular projections being separated by a gap; a circular test coupon disposed in said gap and held by said first and second annular projections; a valve in fluid communication with said channel of said coolant ring; and a source of liquid coolant in fluid communication with said valve. ### Claim 17 (depends on 16) The test system as recited in claim 16, wherein said test coupon has a hole in the center and an outer circumference, said test coupon comprising an inner circumferential portion adjacent said hole and an outer circumferential portion adjacent said outer circumference, and wherein said test system further comprises first and second reinforcing rings respectively bonded to opposite surfaces of said outer circumferential portion of said test coupon. ### Claim 18 (depends on 17) The test system as recited in claim 17, further comprising first and second heat sink disks which are thermally coupled to respective surfaces of said inner circumferential portion of said test coupon. ### Claim 19 (depends on 16) The test system as recited in claim 16, wherein said coolant ring comprises a base and a top coupled to each other by a plurality of fasteners.