# US 9,352,329 B2 · Modularized system and method for urea production using a bio-mass feedstock

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- Number: US 9,352,329 B2
- Document ID: US9352329B2
- Status: Granted
- Kind: B2
- Application number: 14/143,890
- Filed: 2013-12-30
- Published: 2014-08-07
- Granted: 2016-05-31
- Earliest claimed: 2008-08-12
- Assignees: 4A Technologies, LLC
- Applicants: 4A Technologies, LLC
- Inventors: Terry R. Collins; James L. Simonton; Mario G. Beruvides; Jessie Lozada; Ernesto Iznaga
- Web page: https://patentgrep.com/patent/US9352329B2

## CPC

- C07C 273/10: combined with the synthesis of ammonia
- B02C 19/0056: {specially adapted for specific materials not otherwise provided for}
- B02C 21/00: Disintegrating plant with or without drying of the material (for grain B02C9/04)
- B03B 9/061: {the refuse being industrial}
- C10J 3/72: Other features
- C10J 3/82: Gas withdrawal means
- C10L 5/363: {Pellets or granulates}
- C10L 5/44: on vegetable substances
- C10J 2300/0903: Feed preparation
- C10J 2300/0906: Physical processes, e.g. shredding, comminuting, chopping, sorting
- C10J 2300/0916: Biomass
- C10J 2300/1668: to urea; to ammonia
- Y02E 50/10: Biofuels, e.g. bio-diesel
- Y02E 50/30: Fuel from waste, e.g. synthetic alcohol or diesel
- Y02P 20/145: the feedstock being materials of biological origin
- C07C: ACYCLIC OR CARBOCYCLIC COMPOUNDS
- B02C: CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN ({household tools and machines for pulverising foodstuffs, e.g. coffee and spice mills A47J42/00; pharmaceutical mortars A61J3/02; mechanical processing of refuse and garbage B03B9/06; dressing mould materials by grinding B22C5/04}; obtaining metallic powder by crushing, grinding or milling B22F9/04; {recovery of plastics by disintegrating B29B17/00; crushing raw materials in starch making C08B30/02; beaters for papermaking D21D1/02; crushing devices specially for transport in mines E21F13/002; slag crushing devices F23J1/00; fuel milling devices in combustion apparatus F23K1/00; household devices for crushing coal F24B15/02; ice disintegrating devices F25C5/02})
- B03B: SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- C10J: PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES (synthesis gas from liquid or gaseous hydrocarbons C01B; underground gasification of minerals E21B43/295); CARBURETTING AIR OR OTHER GASES
- C10L: FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- Y02E: REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02P: CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

## Abstract

A modular system and method for producing urea from bio-mass includes means and steps for “homogenizing” a biomass feedstock stream having components with different bulk density BTU content into a stream having a consistent bulk density BTU content. The steps include cleaning the incoming bio-mass feedstock stream to remove non-organic matter, blending the cleaned bio-mass feedstock stream to obtain a homogeneous blend having a consistent bulk density BTU content, and milling the homogeneous blend bio-mass feedstock stream to a predetermined size no greater than 12 mm.

## Claims

### Claim 1

A method of preparing a bio-mass feedstock for use in a gasifier, the method comprising the steps of:
(i) cleaning a bio-mass feedstock stream to remove non-organic matter, the bio-mass feedstock stream including a feedstock component having a different bulk density BTU content than at least one other feedstock component, the cleaned bio-mass feedstock stream including no more than 1% foreign matter by weight;
(ii) blending the cleaned bio-mass feedstock stream to obtain a homogeneous blend having a consistent bulk density BTU content;
(iii) milling the homogeneous blend bio-mass feedstock stream to a predetermined size.

### Claim 2 (depends on 1)

A method according to claim 1 wherein the feedstock component and the at least one other feedstock component are from two different sources of bio-mass feedstock.

### Claim 3 (depends on 1)

A method according to claim 1 further comprising the step of routing the milled bio-mass feedstock stream to a gasifier, the routing step providing a feed rate to maintain a constant temperature of the gasifier within a predetermined temperature range.

### Claim 4 (depends on 3)

A method according to claim 3 wherein the constant temperature is held within a range of ±25° C.

### Claim 5 (depends on 3)

A method according to claim 3 wherein the temperature of the gasifier in a range of 800° to 1100° C.

### Claim 6 (depends on 3)

A method according to claim 3 further comprising the step of injecting at least one of a combustible liquid and a combustible solid into the gasifier to maintain the constant temperature.

### Claim 7 (depends on 1)

A method according to claim 1 wherein the predetermined size for the milling step is in a range of 6-10 mm.

### Claim 8 (depends on 1)

A method according to claim 1 wherein the predetermined size for the milling step is no greater than 12 mm.

### Claim 9 (depends on 1)

A method according to claim 1 further comprising the step of pelletizing the homogeneous blend bio-mass feedstock stream to a uniform size prior to the milling step.

### Claim 10 (depends on 1)

A method according to claim 1 further comprising the step of drying the bio-mass feedstock stream after the milling step to a moisture content of less than or about 15% by weight.

### Claim 11 (depends on 10)

A method according to claim 10 wherein the dried bio-mass feedstock stream has a moisture content in a range of 6 to 12% by weight.

### Claim 12 (depends on 10)

A method according to claim 10 wherein the dried bio-mass feedstock stream has a moisture content no greater than 10% by weight.
