Method for producing electrode material for lithium ion batteries
AssigneeShowa Denko K.K.
InventorsMasataka Takeuchi, Yuuichi Kamijou, Yoshiyuki Nishimura, Ryusuke Miura, Takayuki Fukai, Chiaki Sotowa
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AssigneeShowa Denko K.K.
InventorsMasataka Takeuchi, Yuuichi Kamijou, Yoshiyuki Nishimura, Ryusuke Miura, Takayuki Fukai, Chiaki Sotowa
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A method for producing a graphie material for an electrode material for lithium ion batteries, including a step for exothermically graphitizing a carbon material by directly passing an electric current therethrough. The carbon material has an compact powder resistivity of 0.4 Ω·cm or less when compressed to a density of 1.4 g/cm3, has an angle of repose in the range of 20° to 50° inclusive, and has a particle size (D90) in the volume-based particle size distribution measured using laser diffraction of 120 μm or less. The average surface interval (d002) of a surface (002) of the carbon material after graphitization, measured using x-ray diffraction, is in the range of 0.3354 nm-0.3450 nm inclusive.
A method of producing a graphite material for an electrode material for a lithium ion battery, the method including a graphitizing step of directly passing an electric current through a carbon material from an electrode in direct contact with the carbon material to cause the material to generate heat, in which carbon material 1 before the graphitization has a compact powder resistivity of 0.4 Ω·cm or less when compressed to a density of 1.4 g/cm3, has an angle of repose of 20° or more and 50° or less, and has a particle size D90 of 120 μm or less in a volume-based particle size distribution measured by a laser diffraction method, and carbon material 2 after the graphitization has an average interplanar spacing d002 of a (002) plane measured by an X-ray diffraction method of 0.3354 nm or more and 0.3450 nm or less, in which a rectangular parallelepiped furnace body made of ceramic bricks and having an opening in an upper portion thereof is used in the graphitizing step,
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