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US 9,175,101 B2Granted
Precursor for polyolefin catalyst
AssigneeReliance Industries Limited
InventorsUmesh Makwana, Ajay Kothari, Bhavesh Desai, Virendrakumar Gupta
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Abstract
The present invention provides titanium based precursor for polyolefin catalyst with desired morphology and high particle strength. The of preparation of the precursor in accordance with the present invention obviates the use of iodine.
Claims14
A method for synthesis of a catalyst precursor with controlled morphology;
- said method comprising the following steps:
- reacting predetermined amount of magnesium metal particles with an alcohol at a temperature ranging between 35° C. to 50° C. under agitation to obtain a reaction mixture;
- adding a predetermined amount of titanium tetrachloride to the reaction mixture leading to the evolution of hydrogen from the reaction mixture;
- heating the reaction mixture gradually until the temperature of the mixture reaches to a reflux temperature and refluxing the reaction mixture until the time the evolution of hydrogen from the mixture stops completely;
- increasing the temperature of the reaction mixture to about 100° C. to remove the excess alcohol in the reaction mixture to obtain a precursor and subjecting the same to drying.
2 more elements
Dependencies are inferred from the claim text.