# US 9,082,907 B2 · Neutron detection and collimation

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- Number: US 9,082,907 B2
- Document ID: US9082907B2
- Status: Granted
- Kind: B2
- Application number: 13/894,211
- Filed: 2013-05-14
- Published: 2014-10-09
- Granted: 2015-07-14
- Earliest claimed: 2008-11-19
- Assignees: Nova Scientific, Inc.
- Applicants: Nova Scientific, Inc.
- Inventors: W. Bruce Feller; Paul L. White; William J. S. Zhong
- Web page: https://patentgrep.com/patent/US9082907B2

## CPC

- H10F 77/12: Active materials
- G01T 1/00: Measuring X-radiation, gamma radiation, corpuscular radiation, or cosmic radiation (G01T3/00, G01T5/00 take precedence)
- G01T 3/00: Measuring neutron radiation (G01T5/00 takes precedence)
- H10F: INORGANIC SEMICONDUCTOR DEVICES SENSITIVE TO INFRARED RADIATION, LIGHT, ELECTROMAGNETIC RADIATION OF SHORTER WAVELENGTH OR CORPUSCULAR RADIATION
- G01T: MEASUREMENT OF NUCLEAR OR X-RADIATION (radiation analysis of materials, mass spectrometry G01N23/00; tubes for determining the presence, intensity, density or energy of radiation or particles H01J47/00)

## Abstract

A device includes a neutron-sensitive composition. The composition includes, in weight percent, a non-zero amount of aluminum oxide (e.g., approximately 1% to approximately 3.5% aluminum oxide), greater than 12% (e.g., approximately 12% to approximately 17%) boron oxide, greater than approximately 60% silicon oxide (e.g., approximately 62% to approximately 68% silicon oxide), and a non-zero amount of sodium oxide (e.g., approximately 10% to approximately 14% sodium oxide). The device is capable of interacting with neutrons to form an electron cascade.

## Claims

### Claim 1

A device, comprising:
a neutron detector comprising an electron multiplier in the form of a microchannel plate that comprises a neutron-sensitive composition comprising, in weight percent,
a non-zero amount of aluminum oxide,
approximately 12% to approximately 17% boron oxide,
greater than approximately 60% silicon oxide, and
a non-zero amount of sodium oxide,
wherein the neutron-sensitive composition forms the bulk structure of the microchannel plate, the bulk structure defining a plurality of channels, and wherein the device is capable of interacting with neutrons to form an electron cascade.

### Claim 2 (depends on 1)

The device of claim 1, wherein the boron oxide comprises substantially boron-10 enriched boron oxide.

### Claim 3 (depends on 1)

The device of claim 1, wherein the composition further comprises a non-zero amount of calcium oxide less than approximately 4 weight percent.

### Claim 4 (depends on 1)

The device of claim 1, wherein the composition further comprises a non-zero amount of magnesium oxide less than approximately 3 weight percent.

### Claim 5 (depends on 1)

The device of claim 1, wherein the composition further comprises a non-zero amount of arsenic oxide or antimony oxide less than approximately 0.5 weight percent.

### Claim 6 (depends on 1)

The device of claim 1, wherein the composition further comprises a non-zero amount of lithium oxide less than approximately 2 weight percent.

### Claim 7 (depends on 1)

The device of claim 1, wherein the composition is substantially free of lead.

### Claim 8 (depends on 1)

The device of claim 1, wherein the composition consists essentially of, in weight percent, approximately 1% to approximately 3.5% aluminum oxide, approximately 12% to approximately 17% boron oxide, approximately 62% to approximately 68% silicon oxide, approximately 10% to approximately 14% sodium oxide, approximately 0% to approximately 4% calcium oxide, approximately 0% to approximately 3% magnesium oxide, approximately 0% to approximately 0.5% antimony oxide or arsenic oxide, and approximately 0% to approximately 2% lithium oxide.

### Claim 9 (depends on 8)

The device of claim 8, wherein the boron oxide is substantially boron-10 enriched boron oxide.

### Claim 10 (depends on 1)

The device of claim 1, wherein the channels comprise a conducting and electron emissive surface.

### Claim 11 (depends on 1)

The device of claim 1 in which the device is configured to detect the electron cascades in the channels to construct an image.

### Claim 12

A device, comprising:
a neutron detector comprising an electron multiplier in the form of a microchannel plate that comprises an input electrode, a glass plate, and an output electrode, the glass plate comprising a neutron-sensitive composition comprising, in weight percent,
a non-zero amount of aluminum oxide,
approximately 12% to approximately 17% boron oxide,
greater than approximately 60% silicon oxide, and
a non-zero amount of sodium oxide,
wherein the neutron-sensitive composition forms the bulk structure of the glass plate, the bulk structure defining a plurality of microscopic channels, and wherein the device is capable of interacting with neutrons to form electron cascades in the microscopic channels.

### Claim 13 (depends on 12)

The device of claim 12 in which the boron oxide comprises substantially boron-10 enriched boron oxide.

### Claim 14 (depends on 12)

The device of claim 12 in which the composition further comprises a non-zero amount of calcium oxide less than approximately 4 weight percent.

### Claim 15 (depends on 12)

The device of claim 12 in which the composition further comprises a non-zero amount of magnesium oxide less than approximately 3 weight percent.

### Claim 16 (depends on 12)

The device of claim 12 in which the composition further comprises a non-zero amount of lithium oxide less than approximately 2 weight percent.

### Claim 17 (depends on 12)

The device of claim 12 in which the composition is substantially free of lead.

### Claim 18 (depends on 12)

The device of claim 12 in which the channels comprise a conducting and electron emissive surface.

### Claim 19 (depends on 12)

The device of claim 12 in which the composition consists essentially of, in weight percent, approximately 1% to approximately 3.5% aluminum oxide, approximately 12% to approximately 17% boron oxide, approximately 62% to approximately 68% silicon oxide, approximately 10% to approximately 14% sodium oxide, approximately 0% to approximately 4% calcium oxide, approximately 0% to approximately 3% magnesium oxide, approximately 0% to approximately 0.5% antimony oxide or arsenic oxide, and approximately 0% to approximately 2% lithium oxide.

### Claim 20

An apparatus, comprising:
a neutron detector comprising:
a microchannel plate that comprises a neutron-sensitive composition comprising, in weight percent,
a non-zero amount of aluminum oxide,
approximately 12% to approximately 17% boron oxide,
greater than approximately 60% silicon oxide, and
a non-zero amount of sodium oxide,
wherein the neutron-sensitive composition forms the bulk structure of the microchannel plate, the bulk structure defining a plurality of channels, and wherein the microchannel plate is capable of interacting with neutrons to form electron cascades in the channels; and
means for applying a DC bias voltage across the channels in the microchannel plate.
