Back to results
US 9,051,244 B2Granted
Depolymerization of lignin using solid acid catalysts
AssigneeCouncil of Scientific and Industrial Research
InventorsParesh Laxmikant Dhepe, Deepa Ayillath Kutteri
Life of this patent
Estimating the term…
Abstract
The invention provides for a process for the depolymerization of lignin in an inert atmosphere to result in substituted phenolic monomer compounds. The process is catalyzed by heterogeneous solid acid catalysts and is carried out in batch or continuous mode.
Claims10
A process for the conversion of lignin to substituted phenolic compounds, said process comprising the steps of:
- i. charging lignin and a catalyst in the ratio ranging between 0.1:1 to 1:0.1 into a reactor followed by charging a solvent, wherein the catalyst consists of a heterogeneous solid acid catalyst;
- ii. optionally flushing the reactor with nitrogen, argon, helium, hydrogen or air;
- iii. adjusting the reactor to operate at atmospheric pressure and heating the reactor to a temperature in the range of 50 to 300° C. with stirring;
- iv. raising the stirring speed to 10 to 2000 rpm after stabilizing at the temperature;
- and
- v. carrying out a reaction for a period in the range of 0.1 to 96 hours to obtain substituted phenolic compounds.
3 more elements
Dependencies are inferred from the claim text.