# US 9,040,611 B2 · Highly loaded concentrate pellets and preparation of the same

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 9,040,611 B2
- Document ID: US9040611B2
- Status: Granted
- Kind: B2
- Application number: 14/276,915
- Filed: 2014-05-13
- Published: 2014-09-04
- Granted: 2015-05-26
- Earliest claimed: 2010-10-08
- Assignees: E-Z Color Corporation
- Applicants: E-Z Color Corporation
- Inventors: Glen Alan Hirschfeld; Craig A. Dunaway; Jeffrey R. Nonekowski
- Web page: https://patentgrep.com/patent/US9040611B2

## CPC

- C09C 3/006: {Combinations of treatments provided for in groups C09C3/04 - C09C3/12}
- B29B 9/10: by moulding the material, i.e. treating it in the molten state
- B29B 9/12: characterised by structure or composition
- C09C 1/3638: {Agglomeration, granulation, pelleting}
- C09C 1/3676: {Treatment with macro-molecular organic compounds}
- C09C 1/3692: {Combinations of treatments provided for in groups C09C1/3615 - C09C1/3684}
- B29B 9/06: in the form of filamentary material, e.g. combined with extrusion
- C08K 5/00: Use of organic ingredients
- C09C: TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES (treatment of materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone C04B14/00, C04B18/00, C04B20/00); PREPARATION OF CARBON BLACK {; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS}
- B29B: PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- C08K: Use of inorganic or non-macromolecular organic substances as compounding ingredients (paints, inks, varnishes, dyes, polishes, adhesives C09)

## Abstract

A highly loaded concentrate pellet composition includes an active ingredient in a concentration of at least about 60% by weight, and a low molecular weight binder in a concentration of up to about 35% by weight. The active ingredient is evenly dispersed in the binder. The binder has a melting point that permits the composition to melt under shear in an extruder. The binder is non-metallocene and non-stearic.

## Claims

### Claim 1

A highly loaded concentrate pellet composition comprising:
an active ingredient selected from the group consisting of: quinacridone dyes, phthalocyanine dyes, dioxazine dyes, azo-type dyes, nickel titanate, titanium dioxide, iron oxide, metal complexes of mono-azo dyes, metal complexes of diazo-dyes, carbon black, cobalt, chrome antimony titanium buff rutile, sodium aluminum sulpho silicate, and manganese chrome antimony titanate, said active ingredient in a concentration of at least 60% by weight; and
a low molecular weight binder in a concentration of up to 35% by weight, the active ingredient evenly dispersed in the binder, wherein the binder is non-metallocene and non-stearic and not one of: homopolymers and copolymers of high and low density polyethylene, high and low density polypropylene, polystyrene, polyoxymethylene, polyethylene terephthalate, polybutylene terephthalate, polymethyl methacrylate, polyether sulfones, polysulfones, polyether ketones, polystyrene copolymers, acrylonitrile-butadiene-styrene terpolymers, or polyamides.

### Claim 2 (depends on 1)

The highly loaded concentrate pellet composition of claim 1, wherein the binder is a wax with a melting point between 120° F. and 250° F.

### Claim 3 (depends on 1)

The highly loaded concentrate pellet composition of claim 1, wherein the concentration of the active ingredient is between 60% and 93% by total weight and the concentration of the low molecular weight binder is between 35% and 7% by total weight, wherein the binder and the active ingredient account for the total weight of the composition.

### Claim 4 (depends on 1)

A highly loaded concentrate pellet composition of claim 1 comprising:
an active ingredient selected from the group consisting of: quinacridone dyes, phthalocyanine dyes, dioxazine dyes, azo-type dyes, nickel titanate, titanium dioxide, iron oxide, metal complexes of mono-azo dyes, metal complexes of diazo-dyes, carbon black, cobalt, chrome antimony titanium buff rutile, sodium aluminum sulpho silicate, and manganese chrome antimony titanate, said active ingredient in a concentration of at least 60% by weight;
evenly dispersed in a low molecular weight binder, the active ingredient in a concentration of at least 60% by weight, and
the low molecular weight binder in a concentration of up to 35% by weight, wherein the binder is non-metallocene and non-stearic and not one of: homopolymers and copolymers of high and low density polyethylene, high and low density polypropylene, polystyrene, polyoxymethylene, polyethylene terephthalate, polybutylene terephthalate, polymethyl methacrylate, polyether sulfones, polysulfones, polyether ketones, polystyrene copolymers, acrylonitrile-butadiene-styrene terpolymers, and polyamides, wherein the pellet has at least partially a geometric shape formed by a die of the extruder, and the pellet is formed by extrusion through the die of the extruder under mechanical pressure.

### Claim 5 (depends on 1)

A method for preparing a highly loaded concentrate pellet composition of claim 1, comprising:
providing an extruder with a die configured to form a pellet having at least partially a geometric shape by extrusion under mechanical pressure;
providing an active ingredient selected from the group consisting of: quinacridone dyes, phthalocyanine dyes, dioxazine dyes, azo-type dyes, nickel titanate, titanium dioxide, iron oxide, metal complexes of mono-azo dyes, metal complexes of diazo-dyes, carbon black, cobalt, chrome antimony titanium buff rutile, sodium aluminum sulpho silicate, and manganese chrome antimony titanate, said active ingredient in a concentration of at least 60% by weight;
providing a low molecular weight binder, wherein the binder is non-metallocene and non-stearic and not one of: homopolymers and copolymers of high and low density polyethylene, high and low density polypropylene, polystyrene, polyoxymethylene, polyethylene terephthalate, polybutylene terephthalate, polymethyl methacrylate, polyether sulfones, polysulfones, polyether ketones, polystyrene copolymers, acrylonitrile-butadiene-styrene terpolymers, or polyamides;
introducing the active ingredient and the low molecular weight binder to the extruder, the active ingredient evenly dispersed in the low molecular weight binder to form a highly loaded concentrate pellet composition, the active ingredient in a concentration of at least 60% by weight, and the low molecular weight binder in a concentration of up to 35% by weight; and
extruding the composition through the die of the extruder pellet to form a pellet having at least partially a geometric shape, wherein the pellet is cohesive and friable as a result of the mechanical pressure of the extruder.

### Claim 6 (depends on 5)

The method of claim 5, further including the step of preblending the active ingredient and the low molecular weight binder prior to the step of extruding the pellets to evenly disperse the active ingredient in the low molecular weight binder.

### Claim 7 (depends on 1)

The highly loaded concentrate pellet composition of claim 1 further comprising at least one additive selected form group consisting of: an ultraviolet light absorber, a light stabilizer, an antioxidant, a flame-retardant, an antibacterial agent, a surface tension reducers, a deodorizing agent, an anti-static agent, an anti-blocking agent, a plasticizer agents, a blowing agent, a fillers, or mixtures thereof.

### Claim 8 (depends on 7)

The highly loaded concentrate pellet composition of claim 7 wherein the additive is the ultraviolet light absorber.

### Claim 9 (depends on 7)

The highly loaded concentrate pellet composition of claim 7 wherein the additive is the antioxidant.