# US 9,040,469 B2 · Lubricant of solid or liquid consistency, exhibiting low coefficient of friction

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- Number: US 9,040,469 B2
- Document ID: US9040469B2
- Status: Granted
- Kind: B2
- Application number: 13/373,653
- Filed: 2011-11-23
- Published: 2012-05-31
- Granted: 2015-05-26
- Earliest claimed: 2010-11-26
- Applicants: Jacek Długołęcki
- Inventors: Jacek Długołęcki
- Web page: https://patentgrep.com/patent/US9040469B2

## CPC

- C10M 129/40: monocarboxylic
- C10M 129/44: containing hydroxy groups
- C10M 2201/041: Carbon; Graphite; Carbon black
- C10M 2201/05: Metals; Alloys
- C10M 2201/065: Sulfides; Selenides; Tellurides
- C10M 2201/066: Molybdenum sulfide
- C10M 2201/103: Clays; Mica; Zeolites
- C10M 2201/105: Silica
- C10M 2203/1025: used as base material
- C10M 2207/126: monocarboxylic
- C10M 2207/128: containing hydroxy groups; Ethers thereof
- C10M 2213/062: Polytetrafluoroethylene [PTFE]
- C10M 2229/02: Unspecified siloxanes; Silicones
- C10N 2010/02: Groups 1 or 11
- C10N 2010/04: Groups 2 or 12
- C10N 2010/06: Groups 3 or 13
- C10N 2020/06: Particles of special shape or size
- C10N 2030/06: Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
- C10N 2050/10: semi-solid; greasy
- C10M: LUBRICATING COMPOSITIONS (well drilling compositions C09K8/02); USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION (mould release, i.e. separating, agents for metals B22C3/00, for plastics or substances in a plastic state, in general B29C33/56, for glass C03B40/02; textile lubricating compositions D06M11/00, D06M13/00, D06M15/00; immersion oils for microscopy G02B21/33)
- C10N: INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

## Abstract

The invention relates to a lubricant in the form of grease or thick lubricating gel or transmission oil, as well as motor or universal oils with a myriad of applications. As a result of its contents presented in the patent application is characteristic of low coefficient of friction ranging from 0.055 to 0.062. As the main component, the contents of the discussed lubricant includes three or four stearates of metals or hydroxistearates of metals, which interact and cause a noticeable reduction of friction drag on the lubricated surfaces. Additionally, these substances may include a number of other solid or liquid elements, which maintain low friction drags and, furthermore, improve the lubricant through increasing its load capacity, antirust characteristics, shear strength, etc. The lubricant made according to the invention underwent comparative tests against other greases and greasing oils, the accounts of which are included in the application as diagrams, descriptions of research tests and examples of the contents of the lubricant products.

## Claims

### Claim 1

A lubricant of solid consistency, exhibiting a low coefficient of friction, ranging from 0.044 to 0.067, with a liquid base and thickeners as solids, containing a mixture of three out of four metal soaps namely lithium-stearate, or alternately lithium-hydroxystearate, in the amount of from 5% to 10% by weight, calcium-stearate, or alternately calcium-hydroxystearate, in the amount of from 4% to 14% by weight, magnesium-stearate in the amount of from 3% to 9% by weight, or aluminum-stearate in the amount of from 3% to 9% by weight, and at the same time containing polytetrafluoroethylene in the amount from 4% to 8% by weight, and aforesaid metal soaps make up from 51% to 80% of the weight of a lubricating composition, while the liquid base ranges respectively from 49% to 20% by weight.

### Claim 2 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains colloidal silicon dioxide in an amount of not more than 4.5% by weight.

### Claim 3 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains soaps and waxes.

### Claim 4 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains talc powder in grains, wherein an overall dimension of each grain is below 35 μm, but more than 2 μm, in an amount of not more than 6.60% by weight.

### Claim 5 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains polytetrafluoroethylene in powder or in a grain consistency, wherein an overall dimension of each grain is below 100 μm, but more than 2 μm, in the amount from 0.09% to 15.25% by weight.

### Claim 6 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains polimethylsiloxane oil of viscosity from 10 cSt to 1000 cSt, measured in temperature of 40° C., in an amount of from 0.29% to 4.8% by weight.

### Claim 7 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains molybdenum disulfide in grain or powder consistency, wherein an overall dimension of each grain is lower than 50 μm, but for up to 10% by weight more than 2 μm, in an amount of from 0.45% to 10% by weight.

### Claim 8 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains tungsten disulfide in grains or powder consistency, wherein an overall dimension of each grain is lower than 20 μm, but for up to 10% by weight more than 2 μm, in an amount of from 0.45% to 10% by weight.

### Claim 9 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains graphite powder in grains, wherein an overall dimension of each grain of the powder is lower than 20 μm, but for up to 10% by weight more than 2 μm, in an amount of from 0.45% to 10% by weight.

### Claim 10 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains copper nuggets, wherein an overall dimension of each nugget is no more than 80 μm, in an amount of up to 18.5% by weight.

### Claim 11 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains nuggets of a bearing alloy made of tin and/or lead of the firmness of not more than 25 Kg/mm2, according to the Brinell HB measurement method, wherein an overall dimension of each nugget is not more than 80 μm, but for up to 10% by weight more than 2 μm, in an amount of up to 18.5% by weight.

### Claim 12 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains nuggets of tin or nuggets of lead wherein an overall dimension of each nugget is less than 80 μm, but more than 2 μm, in an amount of nuggets of tin or nuggets of lead of not more than 18.5% by weight.

### Claim 13 (depends on 1)

The lubricant according to claim 1, wherein the lubricant contains another lubricant as grease or a lubrication gel for transmission in the amount of up to 87% by weight.

### Claim 14

A lubricant of solid consistency, exhibiting the low coefficient of friction, ranging from 0.044 to 0.067, with the liquid base and thickeners as solids, consisting of a mixture of three out of four metal soaps, namely lithium-stearate or alternately lithium-hydroxystearate in the amount of from 5% to 10% by weight, calcium-stearate or alternately calcium-hydroxystearate in the amount of from 4% to 14% by weight, magnesium-stearate in the amount of from 3% to 9% by weight, or aluminum-stearate in the amount of from 3% to 9% by weight, and aforesaid metal soaps make up from 50.91% to 79.91% of the weight of the lubricating composition, while the liquid base ranges respectively from 49.09% to 20.09% by weight and also is characterized by that the lubricant contains at the same time polytetrafluoroethylene PTFE with an overall dimension of the grains below 100 μm, but more than 2 μm, in the amount from 4% to 8% by weight.

### Claim 15 (depends on 14)

The lubricant according to claim 14, wherein the lubricant is applied to reduce frictional resistance between lubricated surfaces.

### Claim 16 (depends on 14)

The lubricant of solid consistency, according to claim 14, made as grease containing the liquid base in the form of heavy paraffin oil in an amount of 59% by weight and 1-5% of lithium-stearate, or alternatively lithium-hydroxystearate, 1-11% of calcium-stearate, or alternatively calcium-hydroxystearate, 1-9% of magnesium-stearate, 1-9% of aluminum-stearate, with contents of said lubricant supplemented with 4-8% of polytetrafluoroethylene PTFE, and 2% of colloidal silicon dioxide SiO2, and the said lubricant having a coefficient of friction of less than 0.065.

### Claim 17 (depends on 14)

The lubricant according to claim 14, made as greasing gel for helix transmissions, characterized by a very thick transmission oil, containing a base in the form of heavy paraffin oil in the amount of 70% of gel's total weight, while other components include 4-8% of polytetrafluoroethylene PTFE, 1-6% of lithium-stearate, or alternatively lithium-hydroxystearate, 1-8% of calcium-stearate, or alternatively calcium-hydroxystearate, 1-4% of magnesium-stearate, 1-4% of aluminum-stearate, and 2% of colloid silicon dioxide SiO2, the said lubricant having the coefficient of friction less than 0.063.

### Claim 18 (depends on 14)

The lubricant according to claim 14, wherein transmission oil is made up of a base in the form of mineral oil in the amount of 78% of its total weight, while other components include 4-8% of polytetrafluoroethylene PTFE, 1-5% of lithium-stearate, or alternatively lithium-hydroxystearate, 1-4% of calcium-stearate, or alternatively calcium-hydroxystearate, 1-3% of magnesium-stearate, 1-3% of aluminum-stearate, and 3% of colloid silicon dioxide SiO2, 2% of molybdenum disulfide MoS2, the said lubricant having the coefficient of friction below 0.061.

### Claim 19 (depends on 5)

The lubricant according to claim 5, wherein the amount of polytetrafluoroethylene PTFE in various embodiments of the lubricating composition is in the established amount.

### Claim 20 (depends on 14)

The lubricant according to claim 14, wherein the lubricant contains soaps and waxes.
