# US 9,039,333 B2 · Discharge system to remove solids from a vessel

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- Number: US 9,039,333 B2
- Document ID: US9039333B2
- Status: Granted
- Kind: B2
- Application number: 12/444,488
- Filed: 2007-09-10
- Published: 2010-06-10
- Granted: 2015-05-26
- Earliest claimed: 2006-10-10
- Assignees: Univation Technologies, LLC
- Applicants: Randall L. Force; Robert G. Aronson; Mark W. Blood; Gerardo Corona; Dung P. Le; W. Scott Hamilton; Thomas A. Maliszewski; William K. Lutz
- Inventors: Randall L. Force; Robert G. Aronson; Mark W. Blood; Gerardo Corona; Dung P. Le; W. Scott Hamilton; Thomas A. Maliszewski; William K. Lutz
- Web page: https://patentgrep.com/patent/US9039333B2

## CPC

- B01J 8/003: {in a downward flow}
- B01J 8/1809: {Controlling processes}
- B01J 2208/00761: Discharging
- B65G 53/36: Arrangements of containers (hoppers B65D3/06; containers in general B65D)
- B65G 53/56: Switches
- B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B65G: TRANSPORT OR STORAGE DEVICES, e.g. CONVEYORS FOR LOADING OR TIPPING, SHOP CONVEYOR SYSTEMS OR PNEUMATIC TUBE CONVEYORS (packaging B65B; handling thin or filamentary materials, e.g. paper sheets or thread, B65H; cranes B66C; portable mobile or lifting or hauling appliances, e.g. hoists, B66D; devices for lifting or lowering goods for loading or unloading purposes, e.g. fork-lift trucks, B66F9/00; emptying bottles, jars, casks, barrels or similar containers, not otherwise provided for, B67C9/00; delivering or transferring liquids B67D; filling or discharging vessels for liquefied, solidified or compressed gases F17C; pipe-line systems for fluids F17D)

## Abstract

A discharge system for removing a solid/gas mixture from a fluidized bed pressure vessel is provided. The system includes a fluidized bed pressure vessel, settling vessels, discharge lines, primary discharge valves, vent lines, primary vent valves, crosstie lines, crosstie valves, and primary exit valves wherein the system is absent a transfer tank, and absent a filter element. The method provides for transferring a solid/gas mixture via a discharge line from the pressure vessel to a settling vessel, wherein gas is separated from the mixture, and the gas is transferred to at least one other settling vessel via a crosstie line. After the solids are transferred out of the settling vessel, the empty vessel then receives gas from other settling vessels in the system.

## Claims

### Claim 1

A discharge system for removing solids from a fluidized bed pressure vessel, the discharge system comprising:
(a) four settling vessels arranged in parallel;
(b) a discharge line fluidly connecting a fluidized bed pressure vessel to at least one of the settling vessels;
(c) a primary discharge valve to control a discharge flow of a fluid mixture to the at least one of the settling vessels, wherein at least two settling vessels are fluidly connected to the fluidized bed pressure vessel through a single common discharge line and a single common primary discharge valve;
(d) a vent line fluidly connecting the fluidized bed pressure vessel and at least one of the settling vessels;
(e) a primary vent valve to control a vent flow through the vent line, wherein at least two settling vessels are fluidly connected to the fluidized bed pressure vessel through a single common vent line and a single common primary vent valve;
(f) a secondary vent valve in series with the primary vent valve between the fluidized bed pressure vessel and at least one settling vessel;
(g) four crosstie lines, wherein at least one crosstie line fluidly connects at least two of the settling vessels;
(h) at least one crosstie valve to control a crosstie flow through the crosstie line; and
(i) a primary exit valve to control an exit flow of the fluid mixture exiting at least one of the settling vessels,
wherein the discharge system is absent a transfer tank, and wherein the plurality of settling vessels are absent a filter element; and
wherein the discharge system comprises a first set of crosstie lines comprising a first and a second of the four crosstie lines, a second set of crosstie lines comprising a third and a fourth of the four crosstie lines, and at least two multi-port valves, wherein the at least two multi-port valves fluidly connect the first set of crosstie lines to the second set of crosstie lines.

### Claim 2 (depends on 1)

The discharge system of claim 1, wherein at least one of the settling vessels further comprises a conical top head.

### Claim 3 (depends on 1)

The discharge system of claim 1, further comprising a solids monitoring device connected to at least one of the settling vessels.

### Claim 4 (depends on 1)

The discharge system of claim 1, further comprising a plurality of secondary discharge valves in series with the primary discharge valve, wherein the primary discharge valve and at least one of the plurality of secondary discharge valves are located between the fluidized bed pressure vessel and at least one of the settling vessels, and wherein both the primary discharge valve and the at least one of the plurality of secondary discharge valves control the discharge flow to the settling vessel.

### Claim 5 (depends on 1)

The discharge system of claim 1, further comprising a secondary exit valve, wherein both the primary exit valve and the secondary exit valve control the exit flow from at least one of the settling vessels.

### Claim 6 (depends on 1)

The discharge system of claim 1, further comprising a dry-gas purge fed to at least one of the settling vessels.

### Claim 7 (depends on 1)

The discharge system of claim 1, further comprising a clean-gas purge fed to the discharge line.

### Claim 8 (depends on 1)

The discharge system of claim 1, wherein the crosstie valve is a flow-controlling type valve.

### Claim 9 (depends on 1)

A method for removing a solid from a fluidized bed pressure vessel using the discharge system of claim 1, said method comprising
(a) filling a first settling vessel with a mixture from the fluidized bed pressure vessel, wherein said mixture comprises a solid and a pressurized gas;
(b) equalizing the first settling vessel with at least a second settling vessel, wherein the pressurized gas is transferred between the first settling vessel and the second settling vessel; and
(c) emptying the first settling vessel.

### Claim 10 (depends on 9)

The method of claim 9, wherein the equalizing comprises repressurization of at least one of the settling vessels.

### Claim 11 (depends on 9)

The method of claim 9, wherein the equalizing comprises depressurization of at least one of the settling vessels.

### Claim 12 (depends on 9)

The method of claim 9, further comprising recycling the pressurized gas transferred between at least one of the settling vessels and the fluidized bed pressure vessel.

### Claim 13 (depends on 9)

The method of claim 9, wherein the equalizing step comprises repressurization and depressurization of at least two of the settling vessels.

### Claim 14 (depends on 9)

The method of claim 9, further comprising equalizing at least one of the settling vessels with at least two of the settling vessels.

### Claim 15 (depends on 9)

The method of claim 9, further comprising the steps of:
(a) providing at least four settling vessels;
(b) first depressurizing the first settling vessel by transferring a first portion of the pressurized gas from the first settling vessel to the second settling vessel after the filling step;
(c) second depressurizing the first settling vessel by transferring a second portion of the pressurized gas from the first settling vessel to a third settling vessel after the first depressurizing step;
(d) emptying the solid out of the first settling vessel after the second depressurizing step;
(e) first repressurizing the first settling vessel by transferring a first return portion of the pressurized gas from the second settling vessel to the first settling vessel after the emptying step; and
(f) second repressurizing the first settling vessel by transferring a second return portion of the pressurized gas from the third settling vessel to the first settling vessel after the first repressurizing step.

### Claim 16 (depends on 15)

The method claim 15, further comprising the steps of:
(a) third depressurizing the first settling vessel by transferring a third portion of the pressurized gas from the first settling vessel to the fourth settling vessel after the second depressurizing step and before the emptying step; and
(b) third repressurizing the first settling vessel by transferring a third return portion of the pressurized gas from the fourth settling vessel to the first settling vessel after the second repressurizing step.

### Claim 17 (depends on 16)

The method of claim 16, further comprising the steps of:
(a) transferring the pressurized gas from the fourth settling vessel to the third settling vessel at least partially concurrently with the first depressurizing step; and
(b) filling the second settling vessel with the mixture from the fluidized bed pressure vessel at least partially concurrently with the second depressurizing step.

### Claim 18 (depends on 17)

The method of claim 17, further comprising the steps of:
(a) emptying the solid out of the fourth settling vessel at least partially concurrently with the second depressurizing step; and
(b) transferring the pressurized gas from the second settling vessel to the third settling vessel at least partially concurrently with the third depressurizing step.

### Claim 19 (depends on 18)

The method of claim 18, further comprising the steps of:
(a) filling the third settling vessel with the mixture from the fluidized bed pressure vessel at least partially concurrently with emptying the first settling vessel;
(b) filling the fourth settling vessel with the mixture from the fluidized bed pressure vessel at least partially concurrently with the second repressurizing step; and
(c) transferring the solid out of the second settling vessel at least partially concurrently with the second repressurizing step.

### Claim 20 (depends on 19)

The method of claim 19, further comprising the steps of:
(a) transferring the pressurized gas from the third settling vessel to the fourth settling vessel at least partially concurrently with the first repressurizing step; and
(b) transferring the pressurized gas from the third settling vessel to the second settling vessel at least partially concurrently with the third repressurizing step.

### Claim 21 (depends on 9)

The method of claim 9, wherein there are always at least two valves closed between the fluidized bed pressure vessel and a downstream vessel, wherein the downstream vessel is downstream of at least one of the settling vessels.

### Claim 22 (depends on 9)

The method of claim 9, further comprising the step of clean-gas purging a discharge line.

### Claim 23 (depends on 9)

The method of claim 9, further comprising the step of clean-gas purging a vent line.

### Claim 24 (depends on 9)

The method of claim 9, further comprising the step of dry-gas purging at least one of the settling vessels.

### Claim 25 (depends on 9)

The method of claim 9, wherein a volume of discharged solid particles filling the first of the settling vessels is at least 95% of an actual volume of the first of the settling vessels or is greater that about 90% of a valved-in volume of the first of the settling vessels.