# US 9,038,643 B2 · Inhibition of sensory irritation during consumption of non-smokeable tobacco products

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- Number: US 9,038,643 B2
- Document ID: US9038643B2
- Status: Granted
- Kind: B2
- Application number: 13/290,768
- Filed: 2011-11-07
- Published: 2012-10-04
- Granted: 2015-05-26
- Earliest claimed: 2010-03-26
- Assignees: Philip Morris USA Inc.
- Applicants: Gerd Kobal; Justin Heynekamp; Timothy B. Langston; Peter Reeh; Munmaya K. Mishra; Jason W. Flora; Tatjana Kichko
- Inventors: Gerd Kobal; Justin Heynekamp; Timothy B. Langston; Peter Reeh; Munmaya K. Mishra; Jason W. Flora; Tatjana Kichko
- Web page: https://patentgrep.com/patent/US9038643B2

## CPC

- A24B 13/00: Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff (reconstituted tobacco products A24B3/14)
- A24B 15/18: Treatment of tobacco products or tobacco substitutes
- A24B 15/282: {by indirect addition of the chemical substances, e.g. in the wrapper, in the case}
- A24B 15/30: by organic substances {(A24B15/281 takes precedence)}
- A24B: MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF

## Abstract

An orally-enjoyable tobacco product includes a portion of smokeless tobacco comprising an active ingredient and either: (1) a collection of tobacco particles at least partially enclosed by a coating comprising a water-soluble non-crosslinked component and a substantially water-insoluble cross-linked component, or (2) a pouch comprising smokeless tobacco enclosed in a water-permeable wrapper. The active ingredient is selected from the group consisting of a mercaptan, camphor, borneol, isoborneol, bornyl acetate, isobornyl acetate, mono-bornyl succinate, mono-isobornyl succinate, mono-bornyl formate, and mono-isobornyl formate. The active ingredient is present in an amount effective to reduce or eliminate the sensory irritation arising from the smokeless tobacco. Also disclosed is a method of making such a product.

## Claims

### Claim 1

A method of making an orally-enjoyable tobacco pouch product, comprising
encapsulating an active ingredient selected from the group consisting of a mercaptan, camphor, borneol, isoborneol, bornyl acetate, isobornyl acetate, mono-bornyl succinate, mono-isobornyl succinate, mono-bornyl formate, and mono-isobornyl formate in a film or coating;
placing an inner filling material containing tobacco in a porous pouch wrapper;
applying the film- or coating-encapsulated active ingredient to a surface of the pouch wrapper; and
forming at least one seam by bonding opposed layers of the porous pouch wrapper such than an unbonded area is formed between the at least one seam and free edges of the opposed layers so as to form an oral pouch product,
wherein the active ingredient is present in an amount effective to reduce or eliminate sensory irritation arising on oral enjoyment of the pouch product.

### Claim 2 (depends on 1)

The method of claim 1, wherein the active ingredient is furfuryl mercaptan.

### Claim 3 (depends on 1)

The method of claim 1, wherein the active ingredient selected is not the mercaptan.

### Claim 4 (depends on 1)

The method of claim 1, wherein: (1) the active ingredient is encapsulated in cyclodextrin; (2) the active ingredient is selected from the group consisting of borneol, isoborneol, bornyl acetate, isobornyl acetate, mono-bornyl succinate, mono-isobornyl succinate, mono-bornyl formate, and mono-isobornyl formate; (3) the amount of the active ingredient is about 500 picog rams to about 2000 picograms; or (4) two or more of (1), (2), and (3).

### Claim 5 (depends on 1)

The method of claim 1, wherein the product comprises about 500 picograms to about 4 milligrams of the camphor, or the product comprises about 2 nanograms to about 20 nanograms of the camphor.

### Claim 6 (depends on 1)

The method of claim 1, wherein the product comprises the collection of tobacco particles at least partially enclosed by a coating, and the coating contains the active ingredient.

### Claim 7 (depends on 1)

The method of claim 1, wherein the product comprises about 500 picograms to about 4 milligrams of the camphor, or the product comprises about 2 nanograms to about 20 nanograms of the camphor.