# US 9,038,416 B2 · Glass-substrate manufacturing method > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 9,038,416 B2 - Document ID: US9038416B2 - Status: Granted - Kind: B2 - Application number: 13/727,219 - Filed: 2012-12-26 - Published: 2013-07-18 - Granted: 2015-05-26 - Earliest claimed: 2011-03-31 - Assignees: AvanStrate Inc. - Applicants: Hiroyuki Kariya - Inventors: Hiroyuki Kariya - Web page: https://patentgrep.com/patent/US9038416B2 ## CPC - C03B 17/067: {combined with thermal conditioning of the sheets} - C03B 17/064: {by the overflow downdraw fusion process; Isopipes therefor} - C03B 25/12: of glass sheets - G02F 1/1303: {Apparatus specially adapted to the manufacture of LCDs} - G02F 1/133302: {Rigid substrates, e.g. inorganic substrates} - Y02P 40/57: Improving the yield, e-g- reduction of reject rates - C03B: MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES - G02F: OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS - Y02P: CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS ## Abstract A glass-substrate manufacturing method which includes a forming step and a cooling step. In the forming step, a molten glass is formed into a sheet glass by a down-draw process. In the cooling step, the sheet glass is cooled. The cooling step includes first, second and third coating steps as defined herein. ## Claims ### Claim 1 A glass-substrate manufacturing method comprising a forming step of forming a molten glass into a sheet glass by a down-draw process, and a cooling step of cooling the sheet glass, wherein: the cooling step includes a first cooling step of cooling the sheet glass at a first average cooling rate until the temperature of a central region of the sheet glass drops to the annealing point, a second cooling step of cooling the sheet glass at a second average cooling rate until the temperature of the central region drops from said annealing point to a temperature 50° C. below the strain point, and a third cooling step of cooling the sheet glass at a third average cooling rate until the temperature of the central region drops from said temperature 50° C. below the strain point to a temperature 200° C. below the strain point; the first average cooling rate is 5.0° C./second or faster; the first average cooling rate is faster than the third average cooling rate; and the third average cooling rate is faster than the second average cooling rate, wherein: the second average cooling rate is from 0.5° C./second to 5.5° C./second; and the third average cooling rate is from 1.5° C./second to 7.0° C./second. ### Claim 2 (depends on 1) The glass-substrate manufacturing method according to claim 1, wherein the first cooling step includes: a first temperature control step in which the temperature of end sections in the width direction of the sheet glass is lower than the temperature of the central region sandwiched between the end sections, and in which the temperature of the central region is kept uniform; and a second temperature control step in which, after the first temperature control step has been performed, the temperature in the width direction of the sheet glass is decreased from a central section of the sheet glass toward the end sections thereof. ### Claim 3 (depends on 2) The glass-substrate manufacturing method according to claim 2, wherein the second cooling step includes a third temperature control step in which a temperature gradient between each said end section and said central section in the width direction of the sheet glass is decreased as the temperature of the sheet glass approaches near the glass strain point. ### Claim 4 (depends on 3) The glass-substrate manufacturing method according to claim 3, wherein the third cooling step includes a fourth temperature control step in which the temperature in the width direction of the sheet glass is decreased from the end sections toward the central section in the width direction of the sheet glass. ### Claim 5 (depends on 2) The glass-substrate manufacturing method according to claim 2, wherein the third cooling step includes a fourth temperature control step in which the temperature in the width direction of the sheet glass is decreased from the end sections toward the central section in the width direction of the sheet glass. ### Claim 6 (depends on 1) The glass-substrate manufacturing method according to claim 1, wherein the second cooling step includes a third temperature control step in which a temperature gradient between each said end section and said central section in the width direction of the sheet glass is decreased as the temperature of the sheet glass approaches near the glass strain point. ### Claim 7 (depends on 6) The glass-substrate manufacturing method according to claim 6, wherein the third cooling step includes a fourth temperature control step in which the temperature in the width direction of the sheet glass is decreased from the end sections toward the central section in the width direction of the sheet glass. ### Claim 8 (depends on 1) The glass-substrate manufacturing method according to claim 1, wherein the third cooling step includes a fourth temperature control step in which the temperature in the width direction of the sheet glass is decreased from the end sections toward the central section in the width direction of the sheet glass. ### Claim 9 (depends on 1) The glass-substrate manufacturing method according to claim 1, wherein the sheet glass cooled by said cooling step has a thermal contraction rate of 100 ppm or less. ### Claim 10 (depends on 1) The glass-substrate manufacturing method according to claim 1, wherein the cooling step further includes a temperature gradient control step of controlling the widthwise temperature gradient of the sheet glass along the flow direction of the sheet glass. ### Claim 11 (depends on 10) The glass-substrate manufacturing method according to claim 10, wherein the sheet glass cooled by said cooling step has a strain value of 1.0 nm or less. ### Claim 12 (depends on 10) The glass-substrate manufacturing method according to claim 10, wherein the sheet glass cooled by said cooling step has a warpage value of 0.15 mm or less. ### Claim 13 (depends on 10) The glass-substrate manufacturing method according to claim 10, wherein the sheet glass cooled by said cooling step has a thickness deviation of 15 μm or less.